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Three new ternary copper complexes: 3.5H2O(1)、 2H2O (2) sand 1.5H2O(3)(phen=1, 10-phenanthroline, tatp=1, 4, 8, 9-tetranitrogen, dppz =dipyrido [3,2-a; 2,3-c]phenazine, Gly-L-Val=Gly-L-Valine), were synthesized characterized by elemental analysis, molar conductivity, IR and UV-Vis spectroscopes.

本文合成了3个新的三元铜配合物：3.5H2O(1)、2H2O(2)和1.5H2O(3)［Gly-L-Val=甘缬二肽，Phen=l，10-邻菲咯琳，TATP=l，4，8，9-四氮三联苯，DPPZ=二吡啶并［3，2-a；2，3-c］吩嗪］。通过元素分析、红外光谱、紫外－可见光谱以及摩尔电导率测定对这些配合物进行了表征。

Results: Caspase-3 mRNA was constitutively expressed at a low level in freshlyisolated CD34+ cells. The expression of caspase-3 mRNA and protein was upregulated when these cellswere first expanded in suspension culture with growth factors for 3 days. However, only the 32 kDa inactivecaspase-3 proenzyme was detected in the freshly isolated CD34+ cells as well as during the first 3 daysexpansion with cytokines.

检测结果显示，Caspase-3mRNA在新鲜分离的脐血CD34+细胞中低水平表达，在细胞因子支持下体外培养3天，扩增的CD34+细胞中Caspase-3mRNA和蛋白质水平表达上调，但在这两种细胞中仅能检测到分子量为32KDa的非活性酶原形式的Caspase-3；随着体外培养时间的延长，在IL-3，IL-6和GM-CSF组合条件下，Caspase-3被激活，可检测到分子量为20KDa的裂解片段。

Numeration data between the groups using chi-square test.Results:Clinical research:(1) Baseline data: Except for gastrointestinal sthenia syndrome andyin/yang syndrome, the two groups of patients in terms of gender, age, smoking,alcohol consumption, medical history, diseased region, NIHSS score, strokeTCM symptom integration and Gelashige Coma Scale score, as compared withno statistical difference (P＞0.05);(2) After treatment: Compared with pretherapy, the NIHSS score and strokeTCM symptom integration of two groups were prominently improved at 14±3days and 21±3 days. But the improvement of stroke TCM symptom integrationof TFXSJN group was superior to that of the control group, the difference wasstatistically significant (P＜0.05);(3) At 21±3 days, TFXSJN group\' s BI Index, SS-QOL score were higher,and NIHSS score were significantly lower than that of control group, withsignificant differences (P＜0.05); There were no significant differencebetween two groups\' score of mRS at 21±3 days (P＞0.05);(4) Adverse reactions:All patients in the two groups during the treatmenthad no adverse reaction.

结果：临床研究：(1)基线资料中，除腑实证及阴阳类证外，两组患者在性别、年龄、吸烟、饮酒、既往病史、病变部位、NIHSS评分、中风中医症征积分及哥拉斯哥昏迷量表评分等方面相比无统计学差异，具有可比性(P＞0.05)；(2)治疗后，两组患者在14±3天，21±3天时的NIHSS评分、中风中医症征积分较治疗前均有所改善(P＜0.05或P＜0.01)，但TFXSJN组患者的中风中医症征改善优于对照组，具有统计学意义P＜0.05(来源：Ae7B9c9cC论文网www.abclunwen.com；(3)21±3天时TFXSJN组患者的BI指数、SS-QOL评分均高于对照组，NIHSS评分明显低于对照组，差异具有显著性(P＜0.05)；21±3天两组的mRS评分无明显差异(P＞0.05)；(4)不良反应：两组患者在治疗期间均未出现明显不良反应。

Other Psionic and Magic Gear: Dorje of firefall (2nd), dorje of charm person (3rd), crystal capacitor [1] (4th-8th), third eye concentrate (4th), cloak of resistance +1 (5th-19th), dorje of knock (6th-7th), crystal capacitor [3] (7th-11th), dorje of invisibility [9th-level manifester] (8th), crystal mask of mindarmor (9th-12th), 3 powerleech pearls (10th, 18th-20th), dorje of whitefire (10th), amulet of natural armor +1 (11th-16th), third eye aware (11th), psionatrix of Psychoportation (11th), gloves of Dexterity +2 (12th-16th), ring of stabilization (12th), crystal capacitor [5] (13th-16th), torc of free will (13th), bracers of armor +2 (14th-20th), dorje of negate psionics (14th-15th, 18th), ring of fire resistance (16th), amulet of natural armor +2 (17th-20th), skin of striking (17th), crystal capacitor [7] (17th- 18th), gloves of Dexterity +4 (17th-18th), amulet of natural armor +3 (19th-20th), gloves of Dexterity +6 (19th-20th), crystal capacitor [9] (19th), cloak of resistance +3 (20th).

其他灵能和魔法装备："落炎术"灵杖(2级)，"魅惑人类"灵杖(3级)，灵容[1](4至8级)，隐匿镶额眼(4级)，+1抗力斗篷(5至19级)，"敲击术"灵杖(6至7级)，灵容[3](7 至11级)，"隐形术"灵杖[显能者等级9](8级)，水晶心防面具(9至12级)，夺能珍珠×3(10级、18至20级)，"苍火"灵杖(10级)，+ 1天生防御护符(11至16级)，知觉镶额眼(11级)，心灵传送灵锥(11级)，+2敏捷手套(12至16级)，稳定戒指(12级)，灵容[5](13至16级)，自由意志项圈(13级)，+2防御护腕(14至20级)，"消解灵能"灵杖(14至15级、18 级)，次级抗火戒指(16级)，+2天生防御护符(17至20级)，反击灵皮(17级)，灵容[7](17至18级)，+4敏捷手套(17至18级)，+3天生防御护符(19至20级)，+6敏捷手套(19至20级)，灵容[9](19级)，+3抗力斗篷(20级)。

A compound 2-(3-hydroxyphenyl)[60] fullerene pyrrolidine was synthesized by the 1,3-dipolar cycloaddition reaction of the fullerene(C60) and azomethine ylide (prepared from glycine and 3-hydroxybenzaldehyde). The product was characterized by UV-Vis,1H-NMR ,FT-IR and MS. The reaction conditions affecting the yields of product were investigated and the optimum reaction conditions with product yield 75%(based on consumed C60) were:molar ratio of C60∶3-hydroxybenzaldehyde:glycine 1∶3∶6,reaction temperature 95℃,reaction time 18h.

利用甘氨酸和3-羟基苯甲醛与C60发生1， 3-偶极环加成反应，合成分离得到了2-(3-羟基苯基)[60]富勒烯吡咯烷，用UV-Vis、1H-NMR、FT-IR、MS等测试手段表征了产物的结构，并通过单因素方法，探讨了反应条件对产物产率的影响，得到最佳工艺条件：反应物摩尔比1∶3∶6，温度95 ℃，反应时间18 h，产物的产率可达75%（以消耗的C60计）。

To be different from the already chloromethylation catalyst, it has a certain amount of moisture wet, which will not produce huge amounts of doughtic cancerogenic chloromethyl methyl ether during and after the reaction.4,4\'-bisbiphenyl, 1,4-bisbenzene, 1,4-bis(chloro- methyl)-2,5-dimethylbenzene, 1,5-bis-2,4-dimethylbenzene, 4-(chlor- omethyl)-1,2-dimethylbenzene, 1,2-bis-4,5-dimethylbenzene, 5,8-bis-1,2,3,4-tetrahydronaphthalene, 3,3\',5-tris-4,4\'-bisbiphenyl and 3,3\', 5,5\'-tetrakis-4,4\'-bisbiphenyl were synth- esized by using this new catalyst. Results indicated that when the reaction temperature was 55～60℃, the reaction time was 12h, the catalyst which consists of the concentration of 80%H_2SO_4, HAc and Lewis acid, the amount of Lewis acid 0.15 mol(nLewis:nbiphenyl=1.5:1), yield of biphenyl chloromethylation product 4,4\'-bis(chrolomethylbiphenyl can reach a maximum 85%.

采用这种催化体系完成了4，4′-二氯甲基联苯、对二氯甲基苯、1，4-二氯甲基-2，5-二甲基苯、1，5-二氯甲基-2，4-二甲基苯、4-氯甲基-1，2-二甲基苯、1，2-二氯甲基-4，5-二甲基苯、5，8-二氯甲基-四氢萘、3，3'，5-三氯甲基-4，4'-二甲基苯和3，3'，5，5'-四氯甲基-4，4'-二甲基苯的合成，结果表明：在反应条件为：反应温度55～60℃，反应时间12h，选择80%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.15mol(和原料比为1.5：1)，反应效果最好，联苯氯甲基化产物(4，4′-二氯甲基联苯)收率为85%；在反应条件为：反应温度70℃，反应时间8h，80%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，苯的氯甲基化产物收(来源：ABd0C论文eded网www.abclunwen.com)率为75%；在反应条件为：在反应条件为：反应温度40℃，反应时间10h，60%H_2SO_4和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，对二甲苯氯甲基化产物(1，4-二氯甲基-2，5-二甲基苯)收率为78.5%；在反应条件为：反应温度35℃，反应时间10h，60%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，间二甲苯氯甲基化产物(1，5-二氯甲基-2，4-二甲基苯)收率为81.5%。

RESULTS: Sixteen compounds, ursolic acid (1), indole-3-carboxaldehyde (2), indole-3-carboxylic acid (3), p-coumaric acid (4), azelaic acid (5), N-trans-feruloyl tyramine (6), blumenol A (7), 2-hydroxy-3-methylanthraquinone (8), rubiadin l-methyl ether (9), rubiadin (10), quercetin (11), luteolin (12), chrysoeriol 6-C-β-boivinopyranosyl-7-O-β-glucopyranoside (13), alternanthin (14), stigmasta-5, 22-dien-3β-ol (15), and α-spinasterol (16) were obtained from the EtOAc extract of Alternanthera philoxeroides.

结果：得到并鉴定了16个化合物，分别为乌苏酸(1)、吲哚-3-甲醛(2)、吲哚-3-甲酸(3)、对-香豆酸(4)、壬二酸(5)、N-反式阿魏酰基酪胺(6)、布卢姆醇A(7)、2-羟基-3-甲基蒽醌(8)、甲基异茜草素-1-甲醚(9)、甲基异茜草素(10)、槲皮素(11)、木犀草素(12)、柯伊利素-6-C-β-波伊文糖基-7-O-β-吡喃葡萄糖苷(13)、莲子草素(14)、豆甾醇(15)和α-菠甾醇(16)。

Results 6 patients with PAP presented with ground-glass opacification of the bilateral lungs on HRCT. Typical chest HRCT scan showed "map-like" lesions in 3 cases and "cobble stone-like" lesions in 3 cases. Multifocal consolidative opacities in the lungs were seen on HRCT in 3 cases. Lung biopsies from 6 patients with PAP revealed a prominent positive periodic acid-Schiff intra-alveolar exudates. There were normal alveolar spetasis in 3 patients while interstitial thickening, fibroblast hyperplasia, interstitial fibrosis in the others.

结果 6例患者在不同层面可见磨玻璃影，其中2例可见小结节影；3例表现为两肺斑片状磨玻璃影与周围肺组织分界清楚，呈地图样改变；3例因磨玻璃影与小叶间隔增厚交织成铺路石样改变；3例可见肺泡实变融合成密度较高的斑片状阴影，1例在肺泡实变区可见&空气支气管征&。6例患者活检肺组织在光镜下显示肺泡腔内充满大量块状或颗粒状嗜伊红物质，PAS染色阳性，AB染色阴性，其中3例肺泡间隔正常，3例肺泡间隔增宽，可见慢性炎性细胞浸润、成纤维细胞增生和胶原沉积。

The results revealed that there was a significant triple linear re-gression relationship between the HPLC peak areas(1×10￣5mm￣2)of theaflavin(TF,x_1),theaflavin-3-gallate(TF3G,X_2)and theaflavin-3,3′-digallate(TF3,3′DG,X_3) and the organoleptic total score for tea qualityY_(totalor taste ...

结果表明，茶黄素（TL，X＿1）、茶黄素－3－没食子酸酯（TF3G，X＿2）和茶黄素－3.3′双没食子酸酯（TF3.3'DG，X＿3）的HPLC峰面积（1×10￣5mm￣2）与红碎茶感官审评品质总分和滋味得分分）之间存在显著的（P＜0.05）三元线性回归关系。

objective:through analyzing the result of physical fitness test of children aged 3～6 years old in fengtai district of beijing,there is a scientific guiding to the next working in the future and an enhancement of physical exercise.methods:according to "the test standard of physical fitness for children aged 3～6 years old",we had the physical fitness test on 9 784 children aged 3～6 years old.the result of test was analyzed by statistics analysis.results:it is eucrasia for physical fitness of children.the percengts of excellent grade,good grade,passing grade and not passing grade are 59.12%,23.69%,13.31%,3.88%,the total percent of excellent grade is in creasing with the increasing of the age of children.there is some imbalance in test of subitem.conclusion:physical fitness test of children can guide to child care scientifically.physical exercise is very important to growth and development of children,we should pay much attention to it.

目的：分析北京市丰台区托幼园所3～6岁儿童体质测试结果，为儿童保健工作作科学指导，促进儿童体格锻炼。方法：应用《北京市3～6岁儿童体质测试标准》对我区9 784名3～6岁儿童进行体质测试，将结果进行统计学分析。结果：丰台区3～6岁儿童体质健康状况良好，综合评价优秀级占59.12％，良好级占23.69％，及格级占13.31％，不及格级占3.88％。总体评级优秀率随年龄增大而增高，小年龄组不及格者明显多于大年龄组。我区儿童各单项测试项目发展存在不平衡。结论：进行体质测试可对儿童保健工作起科学指导作用，体格锻炼对儿童生长发育极为重要。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失