查询词典 2-butene

Goal compound synthesis namely: Take the vanillic acid as outset raw material, obtains 4- hydroxyl - 3- anisole methyl formate with the methyl alcohol reflux conditions, then after the etherification, the nitration, the return to original state, the ring closure response obtains 6- methoxy - 7- animal pen oxygen radical kui zuo lin - 4- alkone, then passes through the chlorination, the substitution aniline, to escape responses again and so on animal pen oxygen radical, etherification to obtain the goal compound; The goal compound and the diethylamine had the amine substitution reaction to obtain TM1, namely 4- benzene amino - 6- methoxy - 7- [2- hydroxyl - 3-(N, N- two ethyl aminos) third oxygen radical] kui zuo lin; Through zuo has the etherification with the Austria niter to respond obtains TM2, namely 4- benzene amino - 6- methoxy - 7- [2- hydroxyl - 3-(2- methyl - 5- nitryl imidazole) third oxygen radical] kui zuo lin.

目标化合物的合成即：以香草酸为起始原料，与甲醇回流条件下得到4-羟基-3-甲氧基苯甲酸甲酯，然后经过醚化、硝化、还原、环合反应得到6-甲氧基-7-苄氧基喹唑啉-4-酮，然后再经氯化、取代苯胺、脱苄氧基、醚化等反应得到目标化合物；目标化合物与二乙胺发生胺取代反应得到了TM1，即4-苯氨基-6-甲氧基-7-[2-羟基-3-丙氧基]喹唑啉；通过与奥硝唑发生醚化反应得到TM2，即4-苯氨基-6-甲氧基-7-[2-羟基-3-(2-甲基-5-硝基咪唑)丙氧基]喹唑啉。

Each of them exhibited sensitive reduction responses of nitryls. It was found that the reduction peak of nitryl of the position 4-nitrate group of 2,4-dinitrophenol showed great difference from that of the position 5-nitrate group of 2,5-dinitrophenol. The difference between the two reduction potentials was as large as 180 mV.

在pH=5.0、0.1mol/LNaAc-HAc缓冲体系中，2，4-二硝基苯酚和2，5-二硝基苯酚在碳纳米管修饰电极上出现灵敏的硝基还原峰，其中2，4-二硝基苯酚分子中四位硝基的还原峰和2，5-二硝基苯酚分子中五位硝基的还原峰显示出明显差异，二者峰电位差达180mV。

Fruit 1.8-1.9 cm, erect when immature; mericarps smooth, with a basal callus, with 0.3-0.4 mm ± patent nonglandular trichomes; rostrum 1.1-1.2 cm, with a 1.9-2.2 mm narrowed apex; stigmatic remains 3.6-3.8 mm.

果1.8-1.9厘米，未发育完全时直立；分果爿光滑，具基疣，有0.3-0.4毫米多少开展的非腺状毛；喙1.1-1.2厘米，带有1.9-2.2毫米狭窄的先端；柱头残余长3.6-3.8毫米。

Culture tender leaves in culture medium of MS+2,4-D1.5mg/L+30g/L suger+0.7% agar pH5.8 for 20 days in darkness at 25℃, and then subculture to induced Ⅱ-type calli. Use forceps cutting the tissue to nubble with 2mm2, and put the tissue into Agrodacterium tumefaciens LBA4404 liquid supplemented with AS 100mg/L,then, co-culture 3 days, resume 7 days in MS+2,4-D1.5mg/L+30g/L suger+500mg/L cef, take to MS+2,4-D1.5mg/L+30g/L suger+100mg/L cef+10.0mg/L kanamycin culture 20 days in darkness. After that to make it polarize in MS+30g/L suger+100mg/L cef+10.0mg/L km. The percentage of km resistant callus was reached max after infection for 45 min, the average is 29.66%. Simultaneity, tender leave callus are infected 5 min by A. tumefaciens liquid in different negative pressure, and kept on 15 min in Agrodacterium tumefaciens liquid without negative pressure. Then screen out resistant callus and obtain transgenic plants. When the negative pressure is -0.05MP the percentage of km resistant callus was reached max, the average rate is 37.5%.

将心叶接种于MS+2.4-D1.5mg/L+30g/L 蔗糖，琼脂0.7%，pH5.8 培养基中25℃暗培养20d 后继代一次，诱导产生Ⅱ型胚性愈伤组织，用镊子将其夹碎成2mm2大小的小块，置入添加100mg/L AS 的根癌农杆菌LBA4404 菌液中，侵染时间为45min，共培养3 天后，转入MS+2.4-D1.5mg/L+30g/L 蔗糖+500mg/L Cef 培养基中恢复7天，再转入MS+2.4-D1.5mg/L+30g/L 蔗糖+100mg/L Cef+10.0mg/L Km 中，遮光培养20d后，置入其MS+30g/L 蔗糖+100mg/L Cef+10.0mg/L Km 分化，卡那霉素抗性愈伤组织获得率在侵染45min 时达到最大值平均为29.66%；同时以甘蔗心叶愈伤组织材料，通过循环水式真空泵，产生负压，设定不同的负压值，在农杆菌菌液中感染5min 后，在负压条件下继续侵染15min 后，筛选出抗性愈伤组织并获得转化植株，其中在负压为-0.05 时转化率达到最大值，其卡那霉素抗性愈伤组织获得率平均为37.5%。

Equipment includes 2 UHV Omicron Nanotechnology SPMs (1 STM/AFM, 1 STM/ESCA and 1 STM/SEM), 5 Vecco AFMs (2 explorers, 1 Nanoman and 1 Picoforce), 2 Vecco SNOMs and 5 desktop SPM systems.

设备包括2个特高压Omicron SPM的纳米技术（1扫描隧道显微镜/，1原子力显微镜扫描隧道显微镜/能谱和1扫描隧道显微镜/扫描电镜），5 Vecco CNET科技资讯网（2探险家，1 Nanoman和1 Picoforce），2 Vecco SNOMs和5桌面扫描探针显微镜系统。

Time results could be concluded as follows: 1 During the sunshine period, the vertical distribution of external surface temperature on different orientations of buildings differs from one another, and the max discrepancy of vertical temperature appears on the external surface of west oriented wall, whose max differences of the vertical temperature are above 2℃ and the standard deviation of the temperature is above 0.6℃; 2 Most of the time from 2 p.m.

通过一段时间内对某栋典型多层板楼建筑外微气候相关参数的监测，其如下：1）在太阳强辐射时间内，不同朝向的外墙外表面温度随高度分布的情况不同，西向外墙表面温度随高度变化幅度最大，其外表面垂直温度的最大温差一般可在2℃以上，标准偏差约在0.6℃以上；2）多数时间内（主要为下午2点左右至次日凌晨），西墙外表面温度以1层最高；3）建筑热外表面可产生诱导上升热气流。

Thecompound 2-1 can also react with CO and DPPB to give osmium vinyl compound 2-4and 2-5,respectively.

这可以看做是[4+1]环化法在合成金属呋喃方面的应用。2-1与CO以及DPPBPh_2P(CH_2_4PPh_2反应分别得到锇乙烯基化合物2-4和2-5。

The bacteria did not directly oxidate SO3(superscript 2-), and the oxidization of Fe(superscript 2+) by the bacteria seemed to be the key step if oxidation of SO3(superscript 2-).

在突变菌株与Fe(上标 2+)共存时，SO3(上标 2-)的氧化速率明显高于化学氧化，且以间接氧化为主，细菌对Fe(上标 2+)的氧化是反应过程的限制步骤。

Dichlorophenoxyacetic acid (2,4-D), a widely used herbicide, was treated by the ozonization technology in the laboratory.During the 2,4-D ozonization, the main categories of intermediates included chloric aromatics, dechlorinated aromatics and organic acids.Some of these intermediates have relatively high toxicity.Therefore, it is crucial to study the kinetics trend of intermediates diversion.

采用臭氧化高级氧化技术对2，4-D（2，4-二氯苯氧乙酸）污染物进行降解，2，4-D降解过程中会产生含氯芳香中间产物、无氯芳香中间产物和有机酸类中间产物，其中部分中间产物具有较高毒性，因此研究2，4-D臭氧化过程中间产物的动力学变化趋势是非常重要的。

Results All cases underwent surgical treatment; of them, local excision, partial pancreatectomy, pancreaticoduodenectomy, internal drainage and biopsy occurred in 14, 7, 3, 2 and 2 cases, respectively. Only 2 cases developed pancreatic fistula.

结果 28例非功能性胰岛细胞瘤术前定位和手术切除，其中14例行局部切除，7例行胰体尾部切除，3例行胰十二指肠切除，2例行囊肿内引流术，2例行活检术；全组术后并发胰瘘2例(7.1%)。

By using competitive adsorption of activated carbom to remove unfavorable influence of carbon in carbonaceous gold concentrate on leaching process, the leaching rate of gold concentrate can be improved to 88% as compared with 10%by direct cyanidation.

本文论述了利用活性炭竞争吸附作用，消除含炭金精矿中炭在浸出过程中的影响，使金精矿的浸出率可由直接氰化的10％提高到88％。

The only thing you're ever gonna be king of is King of the Stupids!

你只配做傻瓜的国王！