查询词典 2-butene

Their chemical structures were characterizd on the basis of spectral and chemical evidences to be: Sarracenin (1), 2-methyl-5-hydroxy-7-O-ethyl caffeate chromome (2), Naringenin(3), 2-methyl-5, 7-dihydroxychromome (4), 2-methyl-6-hydroxyl-cinnamic acid methyl ester (5), eriodictyol (6), quercetin (7), Naringenin-7-O-β-D-glucoside( 8 ), eriodictyol-7-O-α-D-glucoside (9), quercetin-3-O-β-D-glucoside(10). In addition, one compound was abtained from the n-butanol frationk, which was finally identified as Morrosiside(11) by spectral and chemical evidences.

以波谱数据及其理化性质鉴定为：Sarracenin(1)，2-甲基-5-羟基-7-O-咖啡酸乙酯色原酮(2)，柚皮素(3)，2-甲基-5，7-二羟基色原酮(4)，2-甲基-6-羟基苯丙烯酸甲酯(5)，圣草酚(6)，槲皮素(7)，柚皮素-7-O-β-D-葡萄糖苷(Naringenin-7-O-β-D-glucoside)(8)，圣草酚-7-O-α-D-葡萄糖苷(eriodictyol-7-O-α-D-glucoside)(9)，槲皮素-3-O-β-D-葡萄糖苷(quercetin--3-O-β-D-glucoside)(10)；另外从正丁醇萃取部位分离得到1个化合物，以波谱数据和文献对照鉴定为：Morroniside(11)。

The gold nanoparticle has a maximum absorption peak at 532 nm. The chloroauric acid concentrations and the influence of Cu(superscript 2+), Zn(superscript 2+), Ca(superscript 2+), Fe(superscript 3+), Mg(superscript 2+) and Al(superscript 3+) on the determination were examined.

研究了氯金酸用量等因素对体系的影响，优化了试验条件，并对水中Cu(上标 2+)，Zn(上标 2+)，Ca(上标 2+)，Fe(上标 3+)，Mg(上标 2+)，Al(上标 3+)等常见离子进行了干扰试验。

Results: There was no death with operation or in hospital. There were 42 cases (47.2%) with shortdated low Ca syndrome, 12 cases (13.5%) with transitory craked and 2 cases (2.2%) with Chylous fistula.

结果：全组患者无手术及住院期间死亡，短期低钙血症42例(47.2%)，暂时性声音嘶哑12例(13.5%)，乳糜漏2例(2.2%)。

At three months, the latency and wave amplitude of regenerating nerve were 2.74 0.49msx 19.02 2.32mv respectivly in group A, and 2.32 0.46ms, 21.04 1.09mv respectively in group B, there was no statistical difference in both groups, no regenerating nerves were found to bridge the gaps and cicatrices formed, the results could not be acquired.

肌电图测量及分析术后2月电生理检测再生神经的潜伏期及波幅，A组分别为3.37±0.54ms、13.82±1.73mv，B组分别为2.82±0.49ms、17.45±1.51mv，A组低于B组(p＜0.05)，3个月时A组潜伏期及波幅分别为2.74±0.49ms、19.02±2.32mv，B组分别为2.32±0.46ms、21.04±1.09mv，A、B两组无显著性差异(P＞0.05)。C组仅见瘢痕组织，无神经纤维再生连接缺损处，无法进行检测。3。

Using pyridine-2, 6-dicarboxylic acid as starting material, a novel ligand N^2, N^6-bis(3-methyl-pyridine-2-yl)-pyridine-2, 6-dicarboxamide was synthesized, which contained multidentate and large conjugative system.

以吡啶－2，6-二甲酸为原料，合成含有多个共轭体系多齿配体N^2，N^6-二（3-甲基吡啶）－2-取代吡啶－2，6-二甲酰胺；同时制备它与稀土离子Tb和Eu的配合物，并培养出单晶。

A synthesis of 2-pentylidene cyclopentanone starting from cyclopentanone and n-valeraldehyde through aldol condensation, followed by dehydration, was studied, and the yield reached 85.6%. 2-Pentenyl cyclopentanone was prepared in a yield of 95.0% from 2-pentylidene cyclopentanone with a hydrogenation methodology. Through Baeyer-villiger oxidation,δ-decalactone was synthesized in a yield of 63.9% from 2-pentenyl cyclopentanone with hydrogen peroxide.

研究了以正戊醛和环戊酮为起始原料，经羟醛缩合、脱水反应合成2-戊叉环戊酮，产率达到85.6%，2-戊叉环戊酮加氢制备2-戊基环戊酮，产率为95.0%，2-戊基环戊酮在双氧水作用下经Baeyer-villiger氧化重排反应合成δ-癸内酯，反应产率为63.9%，合成δ-癸内酯的总产率为52.0%，气相色谱分析纯度为98.7%。

Results The patients aged 13 - 30 including 2 cases of type Ⅰ,7 cases of type Ⅱ and 1 case of type Ⅲ,had frequent symptoms of dysmenorrheal and abdominal pain （7 cases）, vaginal puruloid secretion （3 cases） and infertility （3 cases）; 10 of them were complicated with double uterus,2 with unicornous uterus, 3 with endometrial cystis; 8 of them were complicated with ipsilatera renal agenesis, 2 with horseshoe kidney; 2 of them were misdiagnosised.

结果患者年龄13-30岁，Ⅰ型2例，Ⅱ型7例，Ⅲ型1例；临床表现为下腹痛和痛经7例，阴道流脓3例，不孕症3例；10例例均合并双子宫，单角子宫2例，内膜囊肿3例；8例合并同侧肾脏缺如，2例合并马蹄肾；误诊2例；治疗以斜膈切开术为主，部分病例同时行内膜囊肿剥除和单角子宫切除。

Two oleanane type triterpenes were isolated from the crude drug Lu Lu Tong , the fruits of Liquidambar formosana and their structures were elucidated as 2α,3β dihydroxy 23 norolean 4(24), 12(13) dien 28 oic acid(1), 2α,3β,23 trihydroxyolean 12(13) en 28 oic acid(2), based on 13 C NMR, DEPT, 1H NMR, 1H 1H COSY, 13 C 1H COSY, IR, MS and elemental analysis.

从生药路路通分离得到2个齐墩果烷骨架的五环三萜类化合物。通过13CNMR，DEPT，1HNMR，2D1H－13CCOSY，2D1H－1HCOSY，IR，MS和元素分析阐明了它们的结构。（1）为2α，3β－二羟基－23－去甲－齐墩果－4（24），12（13）－二烯－28－羧酸，（2）为2α，3β，23－三羟基齐墩果－12（13）－烯－28－羧酸，（1）未见文献报道，（2）是首次从这一植物中分离得

The new process for preparing 4,4"-Diaminostilbene-2,2"-disulfonic acid was characterized by carrying out the catalytic hydrogenation of 4,4"-dinitrostilbene-2,2"-disulfonic acid or its alkali salts in presence of both Pd/C and OVN in water, the amount of OVN ranging from 0.1 to 0.2% by weight of 4,4"-dinitrostilbene-2,2"-disulfonic acid or its alkali salts, yielding 98.7% of desired product with 99.3% purity.

确定了氧化缩合反应的较佳工艺条件，DNS收率达95.2％，纯度达到了99.1％。而在本论文所确定的还原反应最佳条件下，DSD酸的收率可达98.7％，纯度高达99.5％。

2A series of alternating polyamide-imideswith fluorenyl cardo structure was synthesized by "one-pot" polycondensation of cardo diamines,trimellitic anhydride and various aromatic diamines including p-phenylene diamine,m-phenylene diamine, 4,4\'-oxydianiline,3,4\'-oxydianiline,2,2-bis[4-(4-aminophenoxy)phenyl]propane, 2,2-bis[4-(3-aminophenoxy)phenyl]propane respectively using triphenyl phosphite as condensing agents.

采用&一锅法&(One—pot Synthesis)，由Cardo二胺、偏苯三酸酐和不同二胺包括对苯二胺、间苯二胺、4，4\'—二氨基二苯醚、3，4\'—二氨基二苯醚、2，2—双[4—(4—氨基苯氧基苯基]丙烷和2，2—双[4—(3—氨基苯氧基)苯基]丙烷合成了一系列含有芴基Cardo结构的交替聚酰胺酰亚胺。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。