查询词典 2-butene

The linear concentration ranges for γ-aminobutyric acid, valine and leucine were 5.0×10^(-3)-0.12 g/L, 5.0×10^(-3)-0.08 g/L and 5.0×10^(-3)-0.12 g/L, respectively, and the detection limits (S/N=3) were 2.5×10^(-3), 2.5×10^(-3) and 2.6×10^(-3) g/L, respectively. The relative standard deviations of the peak currents of γ-aminobutyric acid, valine and leucine were 2.5%, 4.9% and 3.9%(n=7), respectively.

氨基丁酸、缬氨酸和亮氨酸的线性范围分别为5.0×10^(-3)~0.12、5.0×10^(-3)~0.08和5.0×10^(-3)~0.12 g/L，检出限(S/N=3)分别为2.5×10^(-3)、2.5×10^(-3)、2.6×10^(-3)g/L；7次平行进样峰高的相对标准偏差分别为2.5%、4.9%、3.9%。

Pistil ca. 1.5-2 cm; corolla white with purple spots, tube 3-3.8 cm, abaxial lip ca. 7 mm; petiole 2-6 cm; leaf blade margin weakly serrate to nearly entire, with vermiform sclereids surrounding vascular bundles; involucre 2-2.5 cm in diam.

约的雌蕊1.5-2厘米；花冠白色具紫色斑点，筒部厘米，背面唇约7毫米；叶柄2-6厘米；叶片边缘身体虚弱的有锯齿到近全缘，具蠕虫状的sclereids 围绕维管束；总苞2-2.5厘米直径 3 Hemiboea bicornuta 台湾半蒴苣苔

In this study, sulfate radical concentration from 4 drip water points (PL1, PL2, SH, JG) in the Shihua cave have been monitored for three years, and those from the drip water point was monitored for two years. Drip discharges show three types of response to surface precipitation variations: rapid response, response with associated time-lag and stable. The results show that:(1) SO(superscript 2- subscript 4) concentration in rapid response drip water increases sharply during rain period and has a exponential relationship with drip rate;(2) in the drip water of lag response, SO(superscript 2- subscript 4) concentration has no significant incrcase during rainfall, but they show a increasing trend during a long-term monitoring;(3) SO(superscript 2- subscript 4) concentration at the stable drip site is low and has no obvious change during wet weason.

本文通过对石花洞洞穴4个滴水点（JG， SH， PL1和PL2）硫酸根浓度近3个水文年的分析测定，结果表明：响应降雨快的滴水点滴水SO(上标 2-下标 4)浓度升高幅度最明显，且滴水SO(上标 2-下标 4)浓度与滴率成指数关系；滞后响应降雨的观测点滴水SO(上标 2-下标 4)浓度雨季升高幅度不明显，但在长期观测期间有明显增加的趋势；对降雨没有响应的滴水点，其SO(上标 2-下标 4)浓度低且雨季没有明显变化。

It includes the following steps: extract trivalent iron ion and divalent iron ion in water phase through organic extractant, get predecessor of; absterge it with secondary distilled water for2-3 times and get pure load metal predecessor of organic phase; mix organic phase of Mg2 and Fe3 with mol rate of 1:2 and introduce them into autoclave, add distilled water according to the rate of 3:1 or 4:1 of organic phase and water phase and airproof it, and then mix it fiercely, stripping with hydrothermal method at temperature between 200 degree C and 300 degree C and make them react for 2.5 hours; cool it to the room temperature under natural condition, separate liquid and centrifugalize it, absterge it with absolute alcohol for 2-3 times and dry it at temperature of 50 degree C for 30-180 minutes, then get product of magnesium ferrite.

包括如下步骤：通过有机萃取剂来萃取水相中的三价铁离子和二价镁离子，制得有机相前驱物；用二次蒸馏水洗涤2-3次，获得纯净的负载金属有机相前驱物；按照Mg 2 和Fe 3 摩尔比1∶2将有机相混合均匀后引入高压釜中，按照有机相与水相的比例为3∶1或4∶1加入蒸馏水，密封后，对溶液进行强力搅拌，水热反萃的温度在200-300℃之间反应2.5小时；自然冷却至室温，分液，离心分离，用无水乙醇洗涤2-3次，在50℃下干燥30-180分钟，得铁酸镁产品。

Results The tumors were divided into three types according to the CT findings. Type I: regular, homogeneous density and well-defined,there were 30 patients, included benign mixed tumor(n=29) and adenolymphomas(n=1); Type II:irregular, heterogeneous dentsity, poordefined, there were 15 patients, included benign mixed tumor(n=7), malignant mixed tumor (n=2),adenolymphomas(n=3), hemagioma(n=2),mucoepidermoid carcinoma(n=1). Type III: irregular and could not definded, there were 7 patients, included malignant mixed tumor(n=2), mucoepidermoid carcinoma(n=2), adenoid cystic carcinoma(n=1), malignant lymphoma(n=1), acinic cell carcinoma(n=1). Conclusion CT have important values in location and qualitative analyses of parotid gland.

结果 肿瘤按CT表现分三类：52例患者中，I类30例，形态规则呈类圆形，密度均匀，边缘清楚，除1例腺淋巴瘤外，29例均为良性混合瘤；II类15例，形态不规则，呈分叶状，密度欠均，边界较清或模糊，其中7例良性混合瘤，2例恶性混合瘤，3例腺淋巴瘤，2例血管瘤，1例黏液表皮样癌；III类7例，形态不规则，边缘无法确定，其中恶性混合瘤2例，黏液表皮样癌2例，囊腺癌1例，恶性淋巴瘤1例，腺泡细胞癌1例。

Sepal 5, fu covers with tiles shape is arranged, chang Sucun, corollaceous bell form, funnel form, tall foot butterfly form or earthen jar form, brim ministry is shallow 5 crack or deep 5 crack, rotate when bud or tweezers closes account; Staminal 5, on canister of move unripe Yu Guan, hide inside or appear, pollen bead does not have thorn or aculeate, on ovary, often be a cup of shape or surround for flower disc place of dissension, 1-4 room, every room contains 1-2 bead ovule, style 1-2, post is not cracked or 2 crack, rare 3 crack, or 2-4 is cracked.

萼片5片，覆瓦状排列，常宿存，花冠钟形。漏斗形。高脚蝶形或瓮形，檐部浅5裂或深5裂，芽时旋转或镊合状；雄蕊5枚，着生于冠筒上，内藏或外露，花粉粒无刺或有刺，子房上位，常为杯状或为分裂的花盘所包围，1-4室，每室含1-2粒胚珠，花柱1-2个，柱头不裂或2裂，稀3裂，或2-4裂。

Four soluble poly(p-phenylene vinylene) derivatives with asymmetric alkoxyl substituents, poly (2-methoxy-5-butoxy)-p-phenylene vinylene, poly [2-methoxy-5-(3'-methyl)butoxy]-p-phenylene vinylene, poly (2-methoxy-5-hexyloxy)-p-phenylene vinylene and poly (2-methoxy-5-octoxy)-p-phenylene vinylene, were prepared by dehydrochlorination reaction with using p-hydroxyanisole and alkyl bromide as raw materials.

以对羟基苯甲醚和溴代烷烃为原料，采用强碱诱导的脱氯化氢缩合聚合法合成了四种可溶性不对称烷氧基取代聚对苯乙炔衍生物，分别为聚（2-甲氧基－5-丁氧基）对苯乙炔、聚［2-甲氧基－5-（3'-甲基）丁氧基］对苯乙炔、聚（2-甲氧基－5-己氧基）对苯乙炔和聚（2-甲氧基－5-辛氧基）对苯乙炔。

To further study the chemical constitutes of lipophilic active parts, we prepared Alc95% and Alc50% according to original literature. 20 compounds were isolated by using macroporous resin, silica gel, polyamide, Sephadex LH-20, Rp-18, preparative TLC and preparative HPLC chromato-graphy. The structures of them were elucidated by means of physical and chemical properties, modern spectroscopic analysis techniques—UV、IR、 EI/MS、ESI/MS、〓H-NMR、〓C-NMR、DEPT、HMQC、HMBC. They are nine anthraquinones: chrysophanol (95-1), physcion (95-2), emodin (95-5), aloemodin (95-7), rhein (50-1), sennoside A or B (50-6),ω-hydroxylemodin (95-10), chrysophanol-8-0-β-D-glucoside (95-12), aloemodin-ω-0-β-D-glucoside (95-13); three phenanthaquinones: tanshinone ⅡA (95-3), cryptotanshinone (95-6), tanshinone Ⅰ(95-4); one isoflavone: 7, 3'-dihydroxyl-5' methoxyisoflavone (95-14) and protocaechuic aldehyde (95-9), protocaechuic acid (95-11), astragaloside Ⅳ(50-4), amygdalin (50-5), 2, 3, 5, 4'-tetrahydroxylstilbene-2-0-β-D-glucoside (50-3),-catechin (50-2), cinnamic acid (95-8). Among them, 3'-dihydroxyl-5' methoxyisoflavone (95-14) is a new compound.

经过溶剂萃取、大孔吸附树脂富集、Sephadex LH-20精制、制备TLC及Semi-pre HPLC等手段从中分离了20个化合物，利用理化性质和波谱技术(UV、IR、EI／MS、ESI／MS、〓H-NMR、〓C-NMR、DEPT、HMQC、HMBC)相结合鉴定了它们的结构，分别为9种蒽醌类化合物：大黄酚，大黄素甲醚，大黄素，芦荟大黄素，大黄酸，番泻苷A或B，ω-羟基大黄素(ω-hydroxylemodin)，大黄酚-8-0-β-D-葡萄糖苷(chrysophanol-8-0-β-D-glucoside)，芦荟大黄素-ω-0-β-D-葡萄糖苷(aloemodin-ω-0-β-D-glucoside)；3种菲醌类化合物：丹参酮ⅡA(tanshinoneⅡA)，隐丹参酮，丹参酮Ⅰ(tanshinone Ⅰ)；1种异黄酮：7，3'-二羟基-5'-甲氧基异黄酮（7，3'-dihydroxy-5' methoxyisofla-vone）以及原儿茶醛，原儿茶酸，黄芪甲苷(astragaloside Ⅳ)，苦杏仁苷，2，3，5，4'-四羟基二苯乙烯-2-0-β-D-葡萄糖苷（2，3，5，4'-tetrahydroxylstilbene-2-O-β-D-g1ucoside），Z—儿茶素，桂皮酸。

Quinazolin-4(3H)-ones(1) were conveniently synthesized from anthranilic acids and amidines,which could be chloridized with POCl_3 to obtain 4-chloroquinazolines (2).The reaction of 2 and 1H-pyrazol-3-amine would give two types of products.In the presence of acid or base,the C-N bond would be formed between the 4-position carbon of 2 and the NH_2 of 1H-pyrazol-3-amine.While the C-N bond between the 4-position carbon of 2 and the NH of 1H-pyrazol-3-amine would be formed when Pd catalyst was utilized.

以邻氨基苯甲酸类化合物和脒为原料，可方便地获得喹唑啉-4(3H)-酮类产物(1)，1经POCl_3氯化可到4-氯代喹唑啉化合物(2)。2与3-氨基-1H-吡唑化合物反应可得到两种类型的产物，在酸、碱条件下2的4位碳和3-氨基-1H-吡唑化合物的NH_2发生C-N成键反应；在Pd催化条件下，2的4位碳则和3-氨基-1H-吡唑化合物的环内NH发生C-N成键反应。

(1) The 2% glutaraldehyole pulpotomy has the function of killing bacteria and could cure deep caries and early pulpitis;(2) The curative effects of six months after operation is better than that of three months and of upper jaw is better than that of lower jaw by using 2% glutaraldehyole pulpotomy;(3) The prognosis of 2% glutaraldehyole pulpotomy depends on selecting indication and the patients cooperation in the course of operation;(4) It must be early performed with the root canal therapy that the cases of further developing apicitis, the absorption of root apiex is over 1/3, the pulp necrosis and periapical disease.

(1) 2%戊二醛活髓切断术具有杀菌的功能，对于深龋及早期牙髓炎可以治愈；(2) 2%戊二醛活髓切断术治疗乳磨牙牙髓炎六个月后的疗效明显好于三个月的疗效，上颌组疗效明显好于下颌组；(3) 2%戊二醛活髓切断术的预后取决于适应证的选择及治疗过程中患儿的配合程度；(4)对于进一步发展为根尖炎的病例及根尖吸收超过1/3、牙髓坏死和根尖周有病变者，应及早行根管治疗术。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。