查询词典 2-butene

Results In early stage group, 5 of 60 cases appeared enophthalmos in first week(8.33%), 48(80%)cases appeared in second week, 53(88.33%)cases appeared in third week. No significant difference was found in second week and third week（χ2＝1.563, P＜0.001. There were significant difference between the first week and second week（χ2＝62.484,P＜0.001 ,the first week and third week（χ2＝76.885,P＜0.001）. There was significant linear correlation between expansion of the orbital volume behind the axis of the globe and the degree of enophthalmos（r=0.994,P＜0.001,with each 1.0ml expansion in the orbital volume behind the axis of the globe causing approximately 1.0mm enophthalmos.

结果：早期组60例患者中，5（8.33%）例患者在1周内出现眼球内陷，48（80%）例在2周内出现内陷， 3周时有53（88.33%）例呈现出内陷；2周时出现眼球内陷的例数与1周时有显著性差异（χ2＝62.484， P＜0.001），2周时出现眼球内陷例数与3周时无差异（χ2＝1.563， P＞0.05），1周时出现眼球内陷例数与3周时有显著差异（χ2＝76.885，P＜0.001），后部眶容积增大与眼球内陷的比值约为1.0，两者之间呈正相关（r=0.994，P＜0.001），即后部眶容积每增加1ml，产生1.0mm的眼球内陷。

Three novel rigid compounds 3, 6-bis[2-(4-pyridylethenyl]-9-ethylcarbazole (L~1), 3,6-bis[2-(2-pyridyl)ethenyl]-9-ethylcarbazole (L~2), 3,6-bis[2-(4-pyridyl)ethenyl]-9 -ethylpyridylcarbazole (L~3) were successfully synthesized by Heck reaction, which were fully characterized by elemental analyses, NMR, MS, IR spectra and single X-ray diffraction analysis.

利用Heck偶联反应，成功地合成了三种新型刚性的吡啶基咔唑类化合物：3，6-二[2-(4-吡啶基)乙烯基]-9-乙基咔唑(L~1)，3，6-二[2-(2-吡啶基)乙烯基]-9-乙基咔唑(L~2)和3，6-二[2-(4-吡啶基)吡啶基]-9-乙基吡啶基咔唑(L~3)，通过元素分析、核磁共振谱、质谱、红外光谱和单晶X-射线衍射等分析手段确证了它们的结构。

Sample configurations are 1 AC, 1 Hiper NMC, 1 Hiper ARC, 2 PRI DSPs,-OR- 2 AC, 1 Hiper NMC, 2 Hiper ARC, and 8 PRI DSPs,-OR- 2 AC, 1 Hiper NMC, 2 Hiper ARC, and 14 PRI DSPs.

样品配置1交流，1艾泰NMC，1艾泰弧，2革命制度党的DSP，或- 2交流，1艾泰NMC，2艾泰电弧，革命制度党的DSP和8，或- 2交流，1艾泰NMC，2艾泰弧，革命制度党的DSP和14。

The preparation method comprises the steps as follows: houghite ZnAl-NO3-LDHs is taken as the precursor, ion exchange method is adopted to insert the 2- naphthylamine-1, 5-disulfonic acid to the interlayer of ZnAl-NO3-LDHs, thereby assembling and acquiring the ZnAl-NADA-LDHs of good crystalling phase structure and splendid performance.

超分子结构2-萘胺-1，5-二磺酸插层材料，简写为ZnAl-NADA-LDHs，其分子式为：[Zn 2 1-x Al 3 x 2 ](C 10 H 7 NO 6 S 2 ) 2- x/2 mH 2 O，是以水滑石ZnAl-NO 3 -LDHs为前体，采用离子交换法将2-萘胺-1，5-二磺酸插入到ZnAl-NO 3 -LDHs层间，组装得到晶相结构良好、性能优异的ZnAl-NADA-LDHs。

The patients include 10 patients(20 eyes) of VogtKoyanagiHarada syndrome, 1 patients(2 eyes) of Behcet diseases, 11 patients(21 eyes) of other uveitis, 5 patients (9 eyes) of papolloedema, 2 patients(2 eyes) of choroidal tumor, 2 patients(4 eyes) of, hypotony with macular degeneration, 1 patient(2 eyes) of,Graves diseases, 1 patient (1 eye) of,blunt trauma and 1 patient(1 eye) of uveal effusion syndrome.

其中伏格特-小柳-原田综合征10例20只眼，Behccet病1例2只眼，其他类型葡萄膜炎11例21眼，视盘水肿5例9只眼，脉络膜肿瘤2例2只眼，低眼压性黄斑病变2例4只眼，Graves眼病1例2只眼，眼钝挫伤1例1只眼，脉络膜渗漏综合征1例1只眼。

Results: At five weeks, the radiographically and manually determined fusion rate for autologous bone graft was 50％(4/8animals), compared with 100％ and 50％(8/8 and 4/8 anilmals) for groups in which fusions were done by using allograft and xenograft augumented with rhBMP-2. Xenograft+HA used in posterolateral intertransverse arthrodesis yielded a fusion rate of 0％(0/8 animals).

结果：手动试验示：1、自体髂骨组即对照组融合率为50％：2、各实验组融合率分别为：同种冷冻干燥异体骨+rhBMP-2组为100％；异种冷冻干燥骨+rhBMP-2组为50％；异种冷冻干燥骨+HA组为0％。X软片示：1、自体髂骨组即对照组X线评分均值为2.75分，融合率为62.5％；2、各实验组结果分别为：同种冷冻干燥异体骨+rhBMP-2组X线评分均值为4分，融合率为100％：异种冷冻干燥骨+rhBMP-2组X线评分均值为2.62分，融合率为62.5％。

Racemic backbones 2-amino-2'-hydroxy-6,6'-dimethyl-l,l'-biphenyl la and 2-amino-2'-hydroxy-4,4',6,6'-tetramethyl-l,1'-biphenyl 1b were synthesized from o-methylaniline and 2,4-dimethylaniline via nitration, diazotation/iodination, Ullmann coupling, selective reduction, diazotation/hydrolysis and hydrogenation.

从邻甲苯胺及2，4-二甲基苯胺出发，经过硝化，重氮化-碘代，偶联，单还原，重氮化-水解及还原反应合成了消旋体骨架2-氨基-2'-羟基-6，6'-二甲基-1，1'-联苯1a和2-氨基-2'-羟基-4，4'，6，6'-四甲基-1，1'-联苯1b。

Starting with commercial available tosylmethyl isocyanide and but-2-enoic methyl ester, pyrrolo[2,1-f][1,2,4]triazine derivatives was prepared by twelve-steps process in total yiled of 5.0%~8% via pyrrole and pyrrolo [2,1-f] [1,2,4] triazine ring formation, substitution and amination reactions etc.

本文以简单的对甲基苯磺酰甲基乙腈和反-2-丁烯酸为原料，经过形成吡咯，吡咯并[2，1-f][1，2，4] 三嗪环，取代，酰胺化等等12步反应，合成了结构新颖的吡咯并[2，1-f][1，2，4] 三嗪衍生物，总收率达5%～8%。

The first synthetic route uses 1,2,4-trimethoxybenzene and chloroacetonitrile in forming 2,4,5-trimethoxy-a-chlor-acetophenone under the anhydrous condition, then the intermediate condensates with papaverine forming the core pyrro[2,l-a]isoquinoline, followed by formation and lactonization to form the lactone ring. The second synthetic route uses prepared aldehyde with prepared ethyl nitroacetate by Knoevenagel condensation to obtain 2-Nitro-3-(2,4,5-tris-methoxy-phenyl)-acrylic acid ethyl ester and 2-Nitro-3-(2,4,5-tris-benzyloxy -phenyl)-acrylic acid ethyl ester etal intermediates. The lamellarin skeleton could arise from condensation of the papaverine and these intermediates by Michael reaction, the ester group is provided for subsequent lactonization. The third synthetic route uses coumarin or indan-l,3-dione derivatives and papaverine to form lamellarin under basic conditions.

第一条路线首先从1，2，4-三甲氧基苯出发与卤乙腈作用合成卤代芳酮中间体，然后与罂粟碱反应合成开链片螺素，最后经乙酰化、去保护、成内酯环得到片螺素；第二条路线由制备的芳醛和制备的硝基乙酸乙酯经缩合得到2-硝基-3-芳基丙烯酸乙酯，然后由该中间体与罂粟碱反应，在完成关环的同时也引入酯基，最后去保护、成内酯环得到片螺素；第三条路线是由香豆素或茚二酮出发，经溴代后的中间体与罂粟碱反应，得到片螺素的基本框架。

The mean ADC value of lymphomatous, metastatic and benign lymph nodes was (0.874±0.17)×10~(-3)mm~2/s,(0.98±0.09)×10~(-3)mm~2/s and (1.20±0.10)×10~(-3)mm~2/s. There was statistically different between benign lymph nodes and other groups (P=0.00). When an ADC value of 1.085×10~(-3)mm~2/s was used as a threshold value for differentiating malignant from benign lymph nodes, the best results were obtained with an sensitivity of 87.8% and specificity of 91.3%. 16 of 18 cases (88.9%) were accurately staged in accordance with clinical staging. For 24 patients after chemotheraphy or radiotheraphy, 4 cases were complete remission and WB-DWI was negative. WB-DWI was positive in 14 of 17 cases with recurrent or remnant tumor. For 3 patients with suspected partial remission, WB-DWI indicated necrosis in 2 cases and inactive in 1 case. Repeated WB-DWI examination was performed in 13 cases, tumors were eradicated in 6 cases, improved in 4, expanded in 2. A new colon carcinoma besides its primary lesion was found in 1 case. The results of WB-DWI were all concordant with other clinical tests.

以ADC值1.085×10~(-3)mm~2／s作为诊断恶性淋巴结病变的临界值，敏感性及特异性分别为87.8％和91.3％。88.9％(16／18)患者WB-DWI检查后分期与临床分期一致。24例淋巴瘤患者放化疗后行WB-DWI检查，4例临床疗效为完全缓解，WB-DWI检查均为阴性，17例临床确认有肿瘤复发及明显残留，WB-DWI显示为阳性的14例，另外3例常规影像评价为部分缓解的患者，WB-DWI检查提示2例病灶以坏死液化为主，1例病灶无明显活性。13例淋巴瘤患者行多次WB-DWI检查，发现6例治疗后病灶消失，4例缓解，1例原发病灶缓解，新出现结肠癌，2例淋巴瘤进展，皆与临床相符。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。