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Steam distillation essential oil principal constituent is bornyl acetate, borneol,2,3-dimethyl-bicyclo , hept-2-ene,caryophyllene,camphene,d-d-cadinene,?
水蒸气蒸馏所得的冷杉精油主要成分为:乙酸龙脑酯,龙脑,2,3-二甲基-双环[2.2.1]-庚-2-烯,石竹烯,莰烯,杜松烯,?
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The yield of rosemary oil was 2%-3%. The constituent analysis of rosemary oil showed that the essential oil mainly contains α-pindne, 1, 8-cineole, camphene, camphor, verbenone, borneol, terpinen-4-ol, limonene, and bornyl acetate.
迷迭香精油的得率在2%~3%,主要含有α-蒎烯、1, 8-桉叶素、莰烯、樟脑、马鞭草烯酮、龙脑、4-松油醇、苎烯和乙酸龙脑酸等成分。
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Compareing with essential oil of the steam distillation method and the bensine solvent extraction method through GC-MS analysis .The result showed that:the essential oil principal constituent extracted by benzine is camphene,a-pinene,bornyl acetate, limonene, 1-methyl-4-(1-methylethyl)-1,4-cyclohexadiene, myrcene, caryophyllene, borneol.
对巴山冷杉针叶水蒸气蒸馏和石油醚萃取所得精油的GC-MS 分析对比研究结果表明:石油醚萃取精油主要成分为:莰烯,a-蒎烯,乙酸龙脑酯,柠檬烯,1-甲基-4-异丙基-1,4-环己二烯,月桂烯,石竹烯,龙脑。
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The result showed that there was significant botanical character difference among the three varieties of rosemary; the content of essential oil of Rosmarinus officinalis L is higher than that of Rosmarinus officinalis 'Rex' and Rosmarinus officinalis 'Wood' with 0.80, 0.46 and 0.40 mL(100g)^(-1)FW respectively;α-pinene、1,8-cineole、verbenone、geraniol and borneol were the main compositions of essential oil from Rosmarinus officinalis L, with 27.26%, 20.92%, 11.75%, 5.92% and 5.07% respectively; the major components of essential oil of Rosmarinus officinalis 'Rex' were 1,8-cineole、camphor、borneol、α-pinene and camphene, accounting for 31.07%, 21.66%, 11.98%, 5.36% and 5.34% respectively; in Rosmarinus officinalis 'Wood', camphor、1,8-cineole、bornyl acetate、borneol、α-pineneand camphene were the major compositions with 24.69%, 23.96%, 6.76%, 5.94%, 5.80% and 5.28% respectively.
结果表明:三种迷迭香的植物学性状,如外形、花色等差异显著;迷迭香的精油含有率较高,为0.80mL(100g)^(-1)FW,Rex迷迭香和Wood迷迭香的精油含有率低,分别为0.46和0.40mL(100g)^(-1)FW;迷迭香的主要成分为α-蒎烯27.26%、1,8-桉叶素20.92%、马鞭烯酮11.75%、香叶醇5.92%、龙脑5.07%等,Rex迷迭香精油中1,8-桉叶素31.07%、樟脑21.66%和龙脑11.98%、α-蒎烯5.36%、莰烯5.34%是其主要成分,Wood迷迭香精油的主要成分为樟脑24.69%、1,8-桉叶素23.96%、醋酸龙脑酯6.76%、龙脑5.94%、α-蒎烯5.80%和莰烯5.28%等。
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Results Ten essential characteristic components have been identified in thirteen batches of Amomum villosum samples, and their relative content was (88.15±2.97)%, which are the representative components. The main components were α-pinene, camphene,β-pinene,β-myrcene, limonene, linalol, camphor, isoborneol, borneol and borneol acetate.
结果 13批次阳春砂仁均含有α-蒎烯、茨烯、β-蒎烯、β-月桂烯、柠檬烯、芳樟醇、樟脑、异龙脑、龙脑、乙酸龙脑酯等10个主要特征成分,合计相对含量达(88.15±2.97)%,具有一定代表性。
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By means of GC, GC-MS, GC-IR, the reaction products were investigated and the results showed that there are triylene, camphene, limonene, p-cymene, terpinolene -terpinene,-terpinene,-fenchyl formate, linalyl formate, terpinyl formate, bornyl formate and isobornyl formate containing in the products,and linalyl formate was first discovered in addition reaction of a -pinene and formic acid .The content of the main product terpinyl formate is up to 60.4%,the selectivity is 64.5%.
采用GC、GC-IR、GC-MS等对反应产物进行定量和定性分析,结果表明:微波辐射下α-蒎烯与甲酸的反应产物含有三环烯、莰烯、对-伞花烃、α-松油烯、γ-松油烯、柠檬烯、异松油烯、甲酸葑醇酯、甲酸异龙脑酯、甲酸龙脑酯、甲酸芳樟酯、甲酸松油酯。
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The yield of borneol and isoborneol was 52.93%,and selectivity for borneol was 60.46%at the conditions of programmed temperatures,reaction time 315 min,saponification time 1h,mass part of catalyst 5%,and terpineol:chloroacetic acid 100∶25.
酯化反应采用程序升温,时间315 min,皂化时间1 h。催化剂用量为松节油质量的5%,松节油∶氯乙酸为100∶25时,龙脑得率为52.93%,正龙脑的选择性为60.46%。
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The yield of borneol and isoborneol was 52.93%,and selectivity for borneol was 60.46%at the conditions of programmed temperatures,reaction time 315 min,saponification time 1h,mass part of catalyst 5%,and terpineol:chloroacetic aci...
酯化反应采用程序升温,时间315 min,皂化时间1 h。催化剂用量为松节油质量的5%,松节油∶氯乙酸为100∶25时,龙脑得率为52.93%,正龙脑的选择性为60.46%。
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The yield of product was 56.1% when rare-earth composite solid superacid SO(superscript 2- subscript 4)/ZrO2-CeO2 was used as catalyst at dosage of 3 % of the mass of β-pinene, while mass ratio of borneol to isoborneol in the product reached 46.0:23.2, showing higher borneol selectivity than other catalysts.
当用稀土复合固体超强酸SO(上标 2-下标 4)/ZrO2-CeO2为催化剂,用量3%时,粗龙脑产率为56.1%,但对正龙脑的选择性高于其他催化剂,正、异龙脑比为
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When the amount of SO(superscript 2- subscript 4)/ZrO2 catalyst was 7% of the mass of β-pinene, the yield of product was 62.0%, and the mass ratio of borneol to isoborneol in the product was 13.6:48.7. When the amount of S2O(superscript 2- subscript 8)/ZrO2 catalyst was 7% of the mass of β-pinene, the yield of product was 66.7%, the mass ratio of borneol to isoborneol in the product was 11.5:49.5. Both two catalysts were poor for borneol selectivity.
在上述反应条件下,当催化剂SO(上标 2-下标 4)/ZrO2用量为7%时(以β-蒎烯质量计,下同),粗龙脑产率为62.0%,产品中正、异龙脑比为13.6:48.7;当催化剂S2O(上标 2-下标 8)/ZrO2用量为7%时,粗龙脑产率为66.7%,正、异龙脑比为11.5:49.5;这两种催化剂对正龙脑选择性比较差。
- 更多网络解释与龙脑相关的网络解释 [注:此内容来源于网络,仅供参考]
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dulia;gurjun;keruing bukut:中脉(假)龙脑香木
角状(假)龙脑香木 keruing;gombang | 中脉(假)龙脑香木 dulia;gurjun;keruing bukut | 小肋(假)龙脑香木 keruing kipas;keruing benar
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gurjun:印度(假)龙脑香木
婆罗洲(假)龙脑香木 keruing sindor;keruing;lagan | 印度(假)龙脑香木 gurjun | 尾状(假)龙脑香木 apitong;tailed leaf panau
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gurjun:缠结(假)龙脑香木
休姆(假)龙脑香木 keruing kerukup | 缠结(假)龙脑香木 yany kraat;dau;hieng;gurjun. | 克氏(假)龙脑香木 malapanau;keruing gondol;kanyin pyan;gurjun
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gurjun:克氏(假)龙脑香木
缠结(假)龙脑香木 yany kraat;dau;hieng;gurjun. | 克氏(假)龙脑香木 malapanau;keruing gondol;kanyin pyan;gurjun | 阔翅(假)龙脑香木 broad-winged apitong;keruing;hagakhak
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gurjun;kanyin;yang:陀螺(假)龙脑香木
小瘤(假)龙脑香木 gurjun;eng;in | 陀螺(假)龙脑香木 gurjun;kanyin;yang | 斯里兰卡(假)龙脑香木 Ceylon gurjun;hora
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gurjun;eng;in:小瘤(假)龙脑香木
坦佩(假)龙脑香木 keruing asam | 小瘤(假)龙脑香木 gurjun;eng;in | 陀螺(假)龙脑香木 gurjun;kanyin;yang
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gurjun;keruing;yang:(假)龙脑香木
锐角(假)龙脑香木 keruing markah;keruing beludu | (假)龙脑香木 gurjun;keruing;yang | 附体(假)龙脑香木 keruing;keruing daun berar;lasang
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keruing sindor;keruing;lagan:婆罗洲(假)龙脑香木
东南亚(假)龙脑香木 keruing;keruing bulu;kanju;wrttaung | 婆罗洲(假)龙脑香木 keruing sindor;keruing;lagan | 印度(假)龙脑香木 gurjun
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Dipterocarpus retusus:龙脑香科 东京龙脑香
四数木科 四数木 Teraeles nudifolra 2 | 龙脑香科 东京龙脑香 Dipterocarpus retusus 1 | 龙脑香科 狭叶坡垒 Hopea chinensis 1
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Dryobalanops aromatica:龙脑树 龙脑、冰片
龙胆 龙胆草 Gentiana scabra | 龙脑树 龙脑、冰片 Dryobalanops aromatica | 龙牙草 仙鹤草 Agrimonia pilosa