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Multistep deposition process has been adopted in the preparation of superfine inorganic composite antibacterial powder, Ag~+ as crystal nucleus, packed outside by the hydroxid and phosphate precipitate of Ti and Zr elements etc., The optimal process conditions have been found from one-factor influence tests and multi-factor orthogonal test,and the optimal process conditions were: Ag iron was imported by silver ammine, and then 100ml Titanyl sulphate solution mixing with zirconium sulfate keep hot at 90 ℃ for 30 mins, and the Zr/Ti ratio is 0.15,and Na_2HPO_4 was added in the end.
超细无机复合抗菌粉体的制备采用以Ag~+沉淀物作为晶核,外包裹Ti、Zr等金属的氢氧化物沉淀和磷酸盐沉淀物的多步沉淀工艺,并利用单因素和正交试验法对制备工艺进行了优化,其最佳工艺条件是:Ag~+以银氨络合物引入,沉淀钛锆的反应时间为0.5h,反应温度为90℃,水解反应时体系总液量为100ml、Zr/Ti为0.15,沉淀物经水洗、干燥,于700℃煅烧4.0h;即得最终产品。