- 更多网络例句与苯基乙醇酸相关的网络例句 [注:此内容来源于网络,仅供参考]
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Dimethicone ,Cyclopentasiloxane,Dimethicone/Vinyl Dimethicone Crosspolymer,Polysilicone-11,Glycoproteins,Panax Ginseng Root Extract,Equisetum Arvense Extract,Silica Dimethyl Silylate ,Bisabolol,Tocopheryl Acetate ,Sodium Hyaluronate,Ursolic Acid,Atelocollagen,Sodium Chondroitin Sulfate,Ethylhexyl Methoxycinnamate,Polyglyceryl-2 Tetraisostearate ,Glycerin ,Water,Alcohol,Butylene Glycol ,Lecithin,Xanthan Gum ,Mica,Fragrance ,Benzyl Alcohol,Linalool ,Hydroxycitronellal,Alpha-Isomethyl Ionone ,Amyl Cinnamal,Hexyl Cinnamal,Palm Tree Extract,Geraniol,Benzyl Benzoate,Butylphenyl Methylpropional,Phenoxyethanol,Methylparaben,Isopropylparaben,Butylparaben ,Isobutyl Paraben,Titanium Dioxide,Carmine
地美司康,环戊硅氧烷,聚二甲基硅氧烷/乙烯基聚二甲硅氧烷交联聚合物,聚硅氧烷-11,糖蛋白,人参根萃取,问荆萃取,二甲基甲硅烷基化硅石,没药醇,醋酸盐维他命E,透明质酸钠,熊果酸,去端肽胶原,硫酸盐软骨素,4-甲氧基肉桂酸-2-乙基己基酯,聚甘油-2 四异硬脂酸酯,甘油,水,酒精,丁二醇,卵磷脂,山羊胶,云母,香料,苯甲醇,沉香醇,羟基香茅醛,α异甲基紫罗酮,戊基肉桂醛,己基肉桂醛,棕榈树萃取,香叶醇,苯甲酸苯甲酯,丁苯基甲基丙醛,苯氧乙醇,羟苯甲酯,羟苯丙酯,羟苯丁酯,二氧化钛,胭脂虫红
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After esterification, the ethyl-2-chloro-3-phenylpropionate reacts with diethyl malonate under the catalysis of sodium ethylate, and we obtain the corresponding triethyl ester. The-benzylsuccinic acid is formed by the triethyl ester reacting with concentrate hydrochloric acid and taking place hydrolyzation and decarboxylation reaction at the same time. In order to avoid the formation of cinnamic acid, the sodium ethylate and diethyl malonate must be react sufficiently. The course has simple operation, inexpensive materials and better yield.
具体制备工艺为:首先以L-苯丙氨酸为原料采用重氮化方法得到-2-氯-3-苯基丙酸,再经酯化得到-2-氯-3-苯基丙酸乙酯后在乙醇钠催化作用下和丙二酸二乙酯缩合,发生SN2反应,得到相应的三乙酯,然后经水解和脱羧,得到-苄基丁二酸;在实验中乙醇钠要和丙二酸二乙酯充分反应,避免生成肉桂酸乙酯;该过程操作简单,原料便宜,产率较高,总收率可达到26.8%。
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Process for the manufacture of a dialkylphenylethylmalonatewhich comprises adding to a quantity of sodium which is covered with a hydrocarbon solvent boiling above 100°C, at least a chemically equivalent proportion of methyl, ethyl or a propyl alcohol, subsequently adding an approximately equivalent proportion of a dialkylcarbonate and of an alkyl phenylacetate, the alkyl groups in these two last-mentioned compounds being preferably the same as the alkyl radical of the above –mentioned lower aliphatic alcohol, heating the mixture to induce reaction and continually distilling out the alcohol formed from the reaction zone and finally causing the sodio diethyl phenylmalonate so formed to interact with an ethylating agent.
生产二烷基苯基丙二酸酯的工艺过程:这包括这包括把至少处于化学平衡的甲醇,乙醇或丙醇添加到覆盖着沸点超过一百摄氏度的碳氢化合物溶剂中,接着加入大约相同当量的二烷基碳酸酯和烷基乙酸苯酯,在刚才提到的化合物中,其烷基集团最好是和刚才提到的低级别脂肪族醇相同,然后加热反应混合物从而引导反应的进行,在反应区域通过连续蒸馏移除形成的醇类。最后使所形成的钠代二乙基苯基丙二酸酯和乙基化试剂反应。
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The other for: safrole, sassafras oil, safrole different 82 yuan / kg; 1 - phenyl -2 - propanone 2,500 yuan / kg; 3.4 dioxane methylene diphenyl -2 - propanone 7200 yuan / ton; Piperonal 1,000 yuan / kg; N-acetyl-o-amino benzoic acid 11500 yuan / ton; anthranilic acid 15,500 yuan / ton; Phenylacetate 15,000 yuan / ton; acetic anhydride 9900 yuan / ton; trichloromethane 4100 yuan / ton ; anhydrous ether 8500 yuan / ton; piperidine 58000 yuan / ton; methyl ethyl ketone 10,000 won / ton; sulfate 1,200 yuan / ton; hydrochloride 400 yuan / ton; ethanol 4200 yuan / ton.
另供:黄樟素、黄樟油、异黄樟素82元/公斤;1-苯基-2-丙酮2500元/公斤;3.4 亚甲基二氧苯基-2-丙酮7200元/吨;胡椒醛1000元/公斤;N-乙酰邻氨基苯酸11500元/吨;邻氨基苯甲酸15500元/吨;苯乙酸15000元/吨;醋酸酐9900元/吨;三氯甲烷4100元/吨;无水乙醚8500元/吨;哌啶58000元/吨;甲基乙基酮10000元/吨;硫酸1200元/吨;盐酸400元/吨;无水乙醇4200元/吨。
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The other for: safrole, sassafras oil, safrole different 82 yuan / kg; 1 - phenyl -2 - propanone 2,500 yuan / kg; 3.4 dioxane methylene diphenyl -2 - propanone 7200 yuan / ton; Piperonal 1,000 yuan / kg; N-acetyl-o-amino benzoic acid 11500 yuan / ton; anthranilic acid 15,500 yuan / ton; Phenylacetate 15,000 yuan / ton; acetic anhydride 9900 yuan / ton; trichloromethane 4100 yuan / ton ; anhydrous ether 8500 yuan / ton; piperidine 58000 yuan / ton; toluene 5200 yuan / ton; methyl ethyl ketone 10,000 won / ton; sulfate 1,200 yuan / ton; hydrochloride 400 yuan / ton; anhydrous Ethanol 4200 yuan / ton.
另供:黄樟素、黄樟油、异黄樟素82元/公斤;1-苯基-2-丙酮2500元/公斤;3.4 亚甲基二氧苯基-2-丙酮7200元/吨;胡椒醛1000元/公斤;N-乙酰邻氨基苯酸11500元/吨;邻氨基苯甲酸15500元/吨;苯乙酸15000元/吨;醋酸酐9900元/吨;三氯甲烷4100元/吨;无水乙醚8500元/吨;哌啶58000元/吨;甲苯5200元/吨;甲基乙基酮10000元/吨;硫酸1200元/吨;盐酸400元/吨;无水乙醇4200元/吨。
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In the presence of ethanol- HCl solution, arylamine-HCl and w=37% aqueous formaldehyde solution or the condensation product of arylamine and formaldehyde are directly reacted with ethyl 3-oxo-2-phenylmethylenebutyrate to form l-aryl-2-phenyl-3-carbethoxy-4-piperidone.
2-苯亚甲基-3-丁酮酸乙酯与芳香胺和w=37%甲醛水溶液或芳胺和甲醛的缩合物在氯化氢-无水乙醇存在下可直接发生的Mannich反应,得到1-对位取代芳基-2-苯基-3-羰乙氧基-哌啶-4-酮。
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Then sodium ethoxide was used as base,the nucleophilic substitution of 2-pyrrolidone with the intermediate provided nefiracetam.
以碳酸钠为缚酸剂,摩尔比为1︰1的2,6-二甲基苯胺与氯乙酰氯反应合成了中间体2-氯-N-(2,6-二甲基苯基)乙酰胺;在强碱乙醇钠作用下,2-吡咯烷酮再与2-氯-N-(2,6-二甲基苯基)乙酰胺经亲核取代合成了目标化合物奈非西坦。
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Resolution of benzoin,hydrobenzoin and α- phenethyl alcohol with-phenylglycine based chiral stationary phase(Chirex 3001)in the normal-phase conditions were studied.
正相模式下研究了安息香、氢化安息香及α-苯乙醇在苯基甘氨酸型手性固定相Ch irex 3001上的拆分,探讨了流动相组成及柱温对手性拆分效果的影响。
- 更多网络解释与苯基乙醇酸相关的网络解释 [注:此内容来源于网络,仅供参考]
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Cinnamaldehyde:肉桂醛
产品名称: 肉桂醛(Cinnamaldehyde) 别名: 3-苯基-2-丙烯醛 CAS编号: 104-55-2 产品说明: 理化性质:无色或浅黄色油状液体.露置空气中易氧化成肉桂酸.有强烈的肉桂味,能随水蒸汽挥发.能与乙醇,乙醚,三氯甲烷等油类溶剂相混容.微溶于水,
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phenylethyl isobutyrate:异丁酸苯乙酯
phenylethyl alcohol 苯基乙醇 | phenylethyl isobutyrate 异丁酸苯乙酯 | phenylethyl propionate 丙酸苯乙酯
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butyl oxamate:草酰胺酸丁酯;乙酰胺酸丁酯
丁基邻[草(之上)+叨]基醚;丁基邻甲苯基醚 butyl o-tolyl ether | 草酰胺酸丁酯;乙酰胺酸丁酯 butyl oxamate | 丁氧乙醇 butyl oxitol; butyl glycol