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Then Doripenem came into the market in the July ,2005. We studied the synthesis of Doripemen.Firstly, we synthesized the chemical 2 from the starting material------o-hydroxylphenylacylamine through Reformastky reaction, alkylation, Diekmann reaction, enolization, esterification and etc. Secondly, we synthesized the chemical 3 from L — hydroxylproline through the protection of carboxyl, amidogen and hydroxyl group, reduction by NaBr, SN_2 substitution and Mitsumobu reaction.
我们以水杨酰胺为起始原料，经Reformatsky反应、烷基化、Diekmann环合、烯醇化、酯化等反应合成双环母核2；再从L-羟基脯氨酸出发，经酯化保护羧基、保护氨基、保护羟基、硼氢化还原酯得醇、Sn2取代和Mitsumobu反应等合成巯基侧链3；最后由化合物3经脱保护、水解得硫醇，和化合物2在二异丙基乙基胺的作用下缩合，最后Pd／C催化脱保护，历经16步反应最终得到产物多尼培南。
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Several modified technology of food protein——acylation, phosphorylation, deamidation, glycosylation, cross linking, proteolysis were reviewed.
综述了酰化作用、磷酸化作用、脱氨基作用、糖基化作用、共价交联作用和蛋白水解作用等6种蛋白质改性技术及最新进展，认为用2种或2种以上方法先后对蛋白质改性是当今普遍使用的技术。
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The famciclovir was synthesized from purine by a series of steps by Acylation, Decarboxylation, Reduction ,and so on; Derivatives of these intermediates is described from the 6-chloro- 9H- purin-2-amine as raw materials in different conditions when the iodine and bromide were synthesized with the addition of two intermediate 6-bromo-9H-purin-2-amine and 6-iodo-9H-purin-2-amine; There is elaborated from the main part of a acetophenone, urineaminohydrochloride, phenylhydrazine, ethyl acetoacetate as raw material through a series of reactions to synthetic 3-phenyl-4-formylphenyl pyrazole and 5-chloro-3-methyl-1-phenyl-1H-pyrazole-4-aldehyde two pyrazole aldehyde, and then with 2-amino-6-chlorine-9-(2-methicillin-oxo-co-methyl-4-yl) purine reaction of the two new pyrazole purine Schiff bases.
本论文主是采用以鸟嘌呤为原料，经过一系列的酰基化，脱羧，还原等反应作用下最终得到了产物2-氨基-9-(4-乙酰氧基-3-乙酰氧基甲基丁基)嘌呤；其中的中间体衍生物主要是阐述从以2-氨基-6-氯鸟嘌呤为原料通过在不同的条件下进行溴代与碘代分别合成了另外两种中间体2-氨基-6-溴鸟嘌呤及2-氨基-6-碘鸟嘌呤；还有一部分主要是阐述从以苯乙酮，盐酸氨基脲，苯肼，乙酰乙酸乙酯为原料通过一系列的反应先合成3-苯基-4-醛基吡唑及5-氯-3-甲基-1-苯基-1H-吡唑-4-甲醛这两个吡唑醛，然后再与2-氨基-6-氯-9-(2-甲氧羰基丁酸甲酯-4-基)嘌呤反应得到了两个新型的吡唑嘌呤席夫碱
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Alanine is formed by transamination when an amino group is donated by gutamine to pyruvic acid. It may be deaminated back to pyruvate for use in the KREBS CYCLE.
它通过转氨作用形成，氨基由谷氨酰氨提供给丙酮酸，它还可以脱去氨基重新形成丙酮酸在三羧酸循环中使用。
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ammonolysis：氯化作用
氨ammonia | 氯化作用ammonolysis | 6.氨基乙酰丙酸脱氢酮deltaaminolevulinicacid dehydrtaase;ALAD
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malic acid dehydrogenase：苹果酸脱氢酶
草酰乙酸由NADP-苹果酸脱氢酶(malic acid dehydrogenase)催化,被还原为苹果酸(malic acid,Mal),反应在叶绿体中进行. 但是,也有植物,其草酰乙酸与谷氨酸在天冬氨酸转氨酶(aspartate amino transferase)作用下,OAA接受谷氨酸的氨基,形成天冬氨酸(aspartic acid,
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chitosan：脫乙醯甲殼質
甲壳质脱乙酰后的脱乙酰甲壳质(Chitosan)结构中有多个羟基及氨基等极性基因,因此有极强的水合能力,保湿性好,可保持皮肤的水份. 同时它的氨基可发挥抗菌防臭作用. 日清纺的]モイスキン]为其代表产品. 艾是菊科多年生草本植物,
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deamidation：脱酰胺基
dealwith 研究 | deamidation 脱酰胺基 | deamination 脱氨基作用