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Pyronine B adheres to on the surface of CdS and prevents CdS aggregating, which leads to the decrease of fluorescence quantum yield of CdS. Fluorescence resonance energy transfer happens from CdS to Rhodamine B, Butyl rhodamine B and Rhodamine 6G, respectively. There is a higher FRET efficiency between CdS and Neutral red with the value being 0.282. Moreover, coupling reaction between -NH_2 of Neutral red and -COOH of CdS -TGA leads to red shift of CdS fluorescence spectrum. The reaction also occurs between Safranine T and CdS. At the same time, the Fluorescence of ST is quenched by forming ST -CdS ground state complex. Chapter 6, CdS QDs modified by chitosan and polyethyleneimine can be quenched by Cu~(2+). According to the experimental result, we develop the novel sensor for Cu~(2+).
研究结果,吡啰红与CdS之间作用形式是染料聚集在CdS的表面使得CdS不易聚集,但同时也降低了CdS的发光的量子效率;罗丹明B、罗丹明6G、丁基罗丹明B均与CdS之间存在能量转移,位阻效应使得能量转移效率最高的BRhB的相对荧光强度增大最小;中性红与CdS的能量转移效率更高,同时推测可能使CdS-TGA上的-COOH与部分NR的-NH_2发生偶联导致粒子变大而发生荧光光谱的红移;番红花红与CdS是相互荧光猝灭,可能是ST的-NH_2与CdS-TGA上的-COOH发生偶联使得纳米粒子变大以及二者形成基态复合物的共同作用的影响。
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Bulky and electron-rich MOP-type phosphine ligand 2-ditertbutylphosphino-2'-isopropyloxy- 1,1'-binaphthyl (L1) shows good catalytic activity in palladium-catalyzed α-arylation of 1,3-dicarbonyl compounds.
富电子、大位阻MOP型烷基膦配体2-二叔丁基膦-2'-异丙氧基-1,1'-联萘(L1)在钯催化的1,3-二羰基化合物的α-芳基化反应中显示了较好的催化活性。
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Bulky and electron-rich MOP-type phosphine ligand 2-ditertbutylphosphino-2 -isopropyloxy 1,1 -binaphthyl (L1) shows good catalytic activity in palladium-catalyzed α-arylation of 1,3-dicarbony compounds.
富电子、大位阻MOP型烷基膦配体2-二叔丁基膦-2'-异丙氧基-1,1'-联萘(L1)在钯催化的1,3-二羰基化合物的α-芳基化反应中显示了较好的催化活性。
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Treatment of dials with N-tert-butanesulfinamide, all biaryl dials were successfully converted into the corresponding bis-imines which were then treated with samarium diiodide to afford diamine products. The absolute configurations of all the intramolecular coupling products were determined by X-ray crystallography.
轴手性二醛与N-叔丁基亚磺酰胺缩合得到相应的亚胺,其为一对非对映异构体。N-叔丁基亚磺酰亚胺在二碘化钐条件下得到的偶联产物,经X-衍射也确定了其立体构型。
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Studing on samarium diiodide promoted asymmetric intramolecular reducing coupling reactions, we have made the resolution of the racemic biaryl dials by using enantiomeric N-tert-butanesulfinamine as the resolving reagent successfully and thus obtained a series of axially chiral biaryl dials with high enantiomeric excess.
中文摘要在二碘化钐促进的分子内不对称还原偶联反应中,我们不仅对联芳基二醛底物的合成路线进行了优化,还发现N-叔丁基亚磺酰胺辅基可以作为手性试剂,成功地对联芳基骨架二醛化合物进行拆分,得到高对映体过量的轴手性二醛类化合物。
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A novel macromonomer,polystyrene capped with thienyl group,which can undergos oxidation coupling polymerization,has been synthesized by anionic polymerization of styrene with butyl lithium as the initiator and 3-bromo-thiophene as the terminator.
以丁基锂为引发剂、四氢呋喃为溶剂,在氮气气氛和-78℃下进行苯乙烯阴离子聚合,并加入 3-溴噻吩作为终止剂,从而合成出末端含噻吩基的聚苯乙烯,它可以进行氧化偶联聚合,是一类新的大分子单体。
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In order to obtain versatile ulitity of host molecules, three new chiral calix [4] crown ethers containing aza, thio atoms bearing two chiral sites provided by -cysteine ester were synthesized by the condensation of calix [4] arene diacid dichloride with oligoethylene glycol bridged bis-amino acid methyl ester. All new compounds were characterized by NMR, MS and elemental analysis.
以-半胱氨酸为手性源,利用多甘醇二氯醚在碱性条件下对半胱氨酸巯基进行烷基化反应,成功地合成了多甘醇醚链桥联的半胱氨酸衍生物,醚化反应后,在高度稀释条件下与对叔丁基杯[4]芳烃二乙酰氯进行双功能基缩合反应成功地合成了新型的手性杯[4]含氮、硫杂冠醚,并利用〓H NMR、MS等谱图手段对其结构进行了表征。
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A series of lanthanide complexes (Ln = Er, Nd, Yb) with infrared emission properties were designed and synthesized by using different anionic ligands [1 -phenyl-3-methyl-4-(4-tertbutylbenzoyl)-5-pyrazolone and l-phenyl-3-methyl-4--5-pyrazolone and 2-naphtoyl trifluoroacetone] and netural ligands (2,2-dipyridine, phenanthroline, triphenylphosphine oxide and water). Three crystal structures of these complexes were obtained and structure studied, and the properties of photoluminescence and fluorescent lifetime were studied in detail.
我们通过选用不同的第一配体[1-苯基-3-甲基-4-(4-异丁酰基)-5-吡唑酮,1-苯基-3-甲基-4-(4-叔丁基苯甲酰基)-5-吡唑酮和2-萘基三氟乙酰丙酮]和第二配体(2,2-联吡啶,邻菲啰啉,三苯基氧膦)合成了16个稀土红外配合物(Ln=Er,Nd,Yb),获得了其中三个配合物的单晶结构,研究了这些稀土红外配合物的光致发光和荧光寿命等性质。
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A kind of silica loaded cerium dioxide particles was prepared by the sol-gel method and the heat-resist performance of the silica loaded cerium dioxide particle added silicon rubber materials improved evidently as compared with that of the purely silica added materials.
研究了两种硅烷偶联剂——乙烯基三乙氧基硅烷(A-151)和乙烯基三特丁基过氧硅烷对高硬度硅橡胶性能的影响,比较发现A-151不但可以显著改善高硬度硅橡胶的回弹性,而且使用方便、成本较低。
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Have carried on testing service for nearly 200 hazardous substances, including Asbestos, PAHs, Phthalates, NP/NPEO, AZO, CFC/HCFC/Halons, PVC, PCB, PCT, PCN, CP, Mirex, TPT/TBT/TBTO, Formaldehyde, Heavy metals, can help your products in fully compliance with 'green purchase' request of international buyers.
开展除RoHS以外的近200种有害物质检测业务,包括石棉、多环芳烃、邻苯二甲酸盐、壬基苯酚/壬基苯酚乙氧基化合物、偶氮染料、氟氯烷烃/氢氯氟烷烃/海龙、聚氯乙烯、多氯联苯、多氯三联苯、多氯化萘、短链氯化石蜡、灭蚊灵、三苯基锡类/三丁基锡类/二的氧化物、甲醛、重金属等,涉及范围完全满足各国际买家的&绿色采购&要求。
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glutamic acid:谷胺酸
胶原蛋白的交联反应通常发生在多胜月太链上天冬胺酸(aspartic acid)及谷胺酸(glutamic acid)上之羰基(carboxyl groups)或离胺酸(lysine)及羟基离胺酸(hydroxylysine)上之胺基,但很少发生在羟基上,例如丝胺酸(serine)、羟丁胺酸(threonine)及羟基脯胺酸.
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Heavy metals:重金属
Halons)、聚氯乙烯(PVC)、多氯联苯(PCB)、多氯三联苯(PCT)、多氯化萘(PCN)、短链氯化石蜡(CP)、灭蚊灵(Mirex)、三苯基锡类(TPT)/ 三丁基锡类(TBT)/ 二(三丁基锡)的氧化物(TBTO)、甲醛(Formaldehyde)、重金属(Heavy metals)等,涉及范围完全满
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bivinyl:丁(间)二烯,联乙烯
bivinyl rubber | 丁二烯(基)橡胶 | bivinyl | 丁(间)二烯,联乙烯 | bivitelline | 双卵黄的