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Contents of aconitine, hypaconitine and mesaconitine incrude drug of aconite root were determined by LC-MS.
采用液-质联用方法，测定乌头类不同饮片中乌头碱、次乌头碱和新乌头碱的含量。
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The results showed as follows: 1 Extraction of gelsemium total alkaloids. Total alkaloids were extracted with 95 per cent ethanol. The extract rate was 0.519 per cent and the extract purity were 88.02 per cent and 87.38 per cent; Total alkaloids were extracted with chloroform .The extract rate was 0.416 per cent and the extract purity were 89.02 per cent and 94.52 per cent. 2 Isolation of gelsemium total alkaloids with TLC. Total alkaloids contained five or more alkaloids. The optimal developing agent was chloroform :methanol :ethyl acetate(9:l:0.3),the optimal eluent was methylene chloride:methanol(92:8). 3 Isolation of total alkaloids with column chromatography. Alkaloid A and alkaloid B were obtained, alkaloid B was identified as koumine.
研究结果如下：1、钩吻总碱的提取：用95％的乙醇提取钩吻生物碱提取率为0.519％，其提取物纯度为88.02％、87.35％；用氯仿提取钩吻生物碱提取率为0.416％，其提取物纯度为89.02％、94.52％。2、钩吻总碱的薄层层析分离：总碱中含有5种或5种已上的生物碱；氯仿：甲醇：乙酸乙酯(9：1：0.3)是最佳薄层层析的展开剂；二氯甲烷：甲醇(92：8)是柱层析的最佳洗脱剂。3、钩吻总碱的柱层析分离：共得到两种钩吻生物碱单体成分碱A和碱B，碱B为钩吻素子，碱A可能是钩吻素甲。4、钩吻总碱的急性毒性试验：钩吻总碱小鼠腹腔注射的半数致死量LD_(50是：7.38mg／kg，95％的可信限范围为：6.67mg／kg～7.94mg／kg。
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The method using periwinkle cells to cultivate and produce vinblastine and vincristine can stably realize the industrialized production of vinblastine and vincristine, and the production cost is rather low, the culture period is short, and the production is insusceptible to the natural environment and weather, so the year-round production can be realized.
本发明的方法用长春花细胞培养生产长春碱和长春新碱，可稳定的实现长春碱和长春新碱的工业化生产，并且其生产成本较低，培养周期短，不受自然环境以及气候的影响，可以实现周年生产。
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Result: Glutin could make the absorption of jatrorrhizine, coptisine, berberine and total alkaloids increased by 30%. Tween 80 and arabic gum did not affect the absorption of berberine, but inhibit that of other alkaloids. There had no influence of lecithin on the absorption of alkaloids.
结果：明胶使药根碱、黄连碱、小檗碱和总生物碱的吸收均提高约30%；聚山梨醇酯和阿拉伯树胶对小檗碱的吸收无影响，而抑制其他3种生物碱和总碱的吸收；卵磷脂几乎不影响各生物碱的吸收。
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An alkaline solution containing mercaptides is regenerated in an improved process wherein the alkaline solution to be regenerated containing a suitable oxidation catalyst is contacted with an oxygen-containing solvent which is immiscible with said alkaline solution in a reaction zone comprising a plurality of fibers positioned longitudinally within a conduit, whereby the two liquids are in contact while concurrently flowing through said reaction zone during which the mercaptides contained in the alkaline solution are oxidized to disulfides and are simultaneously extracted from the alkaline solution into the solvent solution.
包含 mercaptides 的碱解决在一个改良的程序被再产生在何处碱的解决被再产生包含一个适当的氧化催化剂与被说反应的碱的解决组成一个纤维的多数地域纵观地放置在一个导管里面的对一个包含氧的溶剂感到不能相混合的一起连络，那里当协同地流动过说的反应地域的时候，这二种液体保持接触在哪一个期间包含在碱的解决 mercaptides 被使氧化到 disulfides 而且同时地从碱的解决到有偿付能力的解决被吸取。
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Secondly, we established the method of HPLC to determine the content of liensinine in order to control the quality of phenol total base of plumula nelumbinis. With the method we compared three different solvent extraction, and the result showed alcohol-acid water-organic solvent was the best solvent extraction.
使用HPLC法对莲子心酚性总碱中的莲心碱进行质量控制，对三种莲子心酚性总碱的提取方法进行了对比，通过三种溶剂法对莲子心总碱进行提取的实验，结果表明，醇一酸水一有机溶剂提取法提取效率最高，总碱提取率达11.25%，莲心碱提取率为1.20%，此方法操作简便，溶媒易得。
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rutaecarpine pharmacological effects and its related mechanism: rutaecarpine the heart positive inotropic, positive changes in the role and the heart protective effect, which with its promotion of calcitonin gene-related peptide release; rutaecarpine alkali have vasodilative and hypotensive effect, its mechanism mainly related to endothelial cells Ca2 +-NO-cGMP pathways and calcitonin gene-related peptide release; rutaecarpine to relax the anal sphincter, gastrointestinal motility inhibition of stress ulcer and ulcerative colitis have therapeutic effect; rutaecarpine on cerebral ischemia-reperfusion injury has a protective effect, which instead of increasing the concentration of calcitonin gene-related peptide-related; rutaecarpine inhibits platelet aggregation and arterial thrombosis; In addition, rutaecarpine Alkali also anti-inflammatory and analgesic, anti-tumor and other pharmacological effects.
综述了吴茱萸次碱的药理作用及其相关机制：吴茱萸次碱对心脏有正性肌力、正性变时作用和心脏保护作用，这与其促进降钙素基因相关肽释放有关；吴茱萸次碱有扩血管和降压作用，其机制主要涉及内皮细胞Ca2+-NO-cGMP途径和降钙素基因相关肽的释放；吴茱萸次碱能松弛肛门内括约肌，抑制胃肠运动，对应激性溃疡和溃疡性结肠炎也有治疗作用；吴茱萸次碱对脑缺血再灌注损伤有保护作用，这与其增加降钙素基因相关肽浓度有关；吴茱萸次碱能抑制血小板聚集和动脉血栓形成；此外，吴茱萸次碱还有抗炎镇痛、抗肿瘤等药理作用。
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The capsaicin in the sample was alkalized with NaOH solution and mixed with phosphotungstic acid and phospho-molybdic acid , the blue heteropoly acid salt has characteristic absorption at 660 nm.
对以辣椒碱为单剂和复配剂制成生物农药中辣椒碱总量的测定条件研究结果表明，含有辣椒碱的生物农药试料，辣椒碱在碱性溶液中与磷钨酸-磷钼酸作用，生成蓝色的磷钨酸–磷钼酸杂多酸盐，在660nm有最大吸收，其吸光度与溶液中辣椒碱的含量成正比。
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Catalytic synthesis of ethyl chloroacetate with phospho-molybdic acid ;2. The capsaicin in the sample was alkalized with NaOH solution and mixed with phosphotungstic acid and phospho-molybdic acid , the blue heteropoly acid salt has characteristic absorption at 660 nm.
对以辣椒碱为单剂和复配剂制成生物农药中辣椒碱总量的测定条件研究结果表明，含有辣椒碱的生物农药试料，辣椒碱在碱性溶液中与磷钨酸-磷钼酸作用，生成蓝色的磷钨酸–磷钼酸杂多酸盐，在660nm有最大吸收，其吸光度与溶液中辣椒碱的含量成正比。
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Chemistry of or denoting or of the nature of or containing a base.
某种碱的、表示某种碱的、具有某种碱的特性或者含有某种碱。
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alkaline：碱的
alkalimetry 碱量滴定法 | alkaline 碱的 | alkaline accumulator 碱性蓄电池
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antalkaline：解碱的,抗碱的
antalkali | 碱性中和剂, 抗碱剂 | antalkaline | 解碱的,抗碱的 | antaphrodisiac | 抑制性欲的药品 镇欲剂
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alkaliferous：含碱的
alkalic?calcic rock sreies 碱钙性岩系 | alkaliferous 含碱的 | alkalimeter 碱度计
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alkaligenous：产碱的
alkaligenous产碱的 | alkalimeter碱定量计 | alkalimetry碱定量法
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alkaligenous;alcaligenous：产碱的
产碱杆菌属 Alkaligenes;Alcaligenes | 产碱的 alkaligenous;alcaligenous | 碱定量计 alkalimeter
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alkaloidal：似碱的
alkaloidal 生物碱的 | alkaloidal 似碱的 | alkalosis 碱中毒
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alkaloidal：生物碱[的]/似碱的
alkaloid /生物碱/植物碱基/ | alkaloidal /生物碱[的]/似碱的/ | alkalosis /碱中毒/
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basophilic：嗜碱的
basophilia 嗜碱性细胞增多 | basophilic 嗜碱的 | basophilic leukemia 嗜碱细胞性白血病
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dibasic：二碱的
dibasic sodium phosphate 磷酸二钠 | dibasic 二碱的 | dibasic 二碱的二元的
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dibasic：二碱的二元的
dibasic 二碱的 | dibasic 二碱的二元的 | dibromotetrafluoroethane 二溴四氟乙烷