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Novel chitosan derivative with long alky groups as the hydrophobic moieties and carboxymethyl groups as the hydrophilic moieties was synthesized. The chemical structure of N-octyl-O, N-carboxymethyl chitosan was characterized via FTIR, 1H NMR and elemental analysis. The physical properties were analyzed with wide angle X-ray diffraction and differential scanning calorimetry.
以天然可生物降解的壳聚糖为原料，通过在壳聚糖6位羟基上引入羧甲基，在2位氨基上引入疏水烷基链，制得N-辛基－O，N-羧甲基壳聚糖两亲性衍生物，分别用FTIR、1H NMR和元素分析等技术对其结构进行表征，用广角X射线衍射和差示扫描量热法对具物理性质进行分析，并考察其在各种溶剂中的溶解性能及其对难溶性药物的增溶能力。
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The bond angle of O-M-O for the two complexes are in excellent agreement with each other.
化合物4和5的差热分析也表明化合物有一个非配位水和两个配位水。
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The results indicate that thermal stabilities and decomposition mechanisms of the title compounds derived from the BDE, Ea and static electronic parameters are basically consistent. Homolysis of the N—NO2 bond is the initial step in the thermolysis of the title compounds, the meta-isomers are more stable than the para-isomers, and the ortho-isomers are the most sensitive.
结果表明，由BDE、Ea和静态电子结构参数推断的标题物热稳定性和热解机理的结论基本是一致的，N-NO2键均裂是标题物的热解引发步骤，间位取代异构体较对位取代异构体稳定，而邻位取代的异构体稳定性最差。
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In the fourth chapter, four new complexes of hydrazide of podophyllic acid with transition metals have been prepared. Elemental analysis, molar conductivity, IR,〓 NMR and TG-DTA were used to characterize them. The results show that general formula of the complexes is M〓(n=0 or 2). The ligand is linked through the carbonyl oxygen and the terminal nitrogen of the hydrazide base to the transition metal ions in bidentate mode.
第四章 合成了四种鬼臼酰肼的过渡金属配合物，通过元素分析、摩尔电导、红外光谱、核磁共振氢谱和热重-差热对配合物进行了表征，研究结果表明，配合物的组成为M〓（n=0或2），配体是通过羰基氧和肼基上的端氮以双齿形式与金属离子配位的。
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It can be concluded that the slipping of phase interfaces or the viscous sliding of grain boundary, dislocation's oscillation, the infinitesimal plastic deformation that was caused by the difference of elastic module and heat expansion coefficient between phases of the alloy yielded the damping of the alloys.
研究表明合金的阻尼是由合金晶界和相界面滑动、位错振荡以及各相的热膨胀系数和弹性模量间差造成的微塑性变形共同造成的。
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The main products of our company are LED-column type digital display transmitter, alarm display converter, polling system alarm instrument, intellectual adjusting instrument, flux integrating controller, Q,D instrument, rack-mounted, wall-mounted, clamp type instruments, flashing alarm instrument, three-phase controllable silicon temperature controller, diffused silicon pressure/fluid level transmitter, capacitance voltage/pressure transmitter, thermocouple, thermo-resistance, bimetal thermometer, onsite thermal calibration devices, automation device.
公司主要生产光柱数字式显示变送仪、显示变送报警仪、巡检变送报警仪、智能调节仪、流量积算控制仪、Q、D型操作器、架装式、墙挂式、卡式仪表、闪光报警器、三相可控硅微处理温度控制柜、扩散硅压力/液位变送器、电容式差压/压力变送器、热电偶、热电阻、双金属温度计，现场热工校验装置、自动化成套设备，可广泛地应用于炼油、化工、建材、轻工、冶金、纺织等行业的温度、压力、流量、液位等参数的自动化监测和控制。
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In the paper, the multidentate carboxylic acid ligands were used to combine with Cd, resulting in the three dimensional MOCPs single crystals—C12H16CdN2O8, with a low temperature hydrothermal synthesis method. The sample was characterized with IR spectra to affirm the organic groups in the frameworks, single-crystal X-ray diffraction to determine the crystal structure and composition of the frameworks, N2 adsorption isotherms at low temperature to measure the specific surface area and pore size distribution, and with TGA/DGA analysis to scale the thermal stability. Furthermore, the dissolution property and the photocatalytic activity of MOCPs under the ultraviolet ray condition were explored.
本文用低温水热合成法，用多齿羧酸配体异烟酸和Cd配位合成出[Cd(C6H4O2N)2(H2O)4]∞三维晶体并进行了表征：采用红外光谱法确认骨架中的有机官能团；用单晶X射线衍射分析法测定MOCPs的晶体结构，并确定其骨架的组成；通过低温氮气吸附等温线测定了其比表面积和孔径分布；以热重分析和差热分析测定材料骨架的热稳定性；测定了晶体的溶解性能；最后以亚甲基蓝为目标降解物，对[Cd(C6H4O2N)2(H2O)4]∞的光催化活性及亚甲基蓝的氧化动力学进行了探索(来源：A2444BC论文网www.abclunwen.com)。
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The complexes were characterized by elemental analysis,UV,IR,TG,NMR and molar conductance measurements.Their formulas were in accordance with C34H32O8N2LnCl·nH2O or 〔(L4)2LnCl·nH2O,Ln=Nd,n=4;Ln=Pr,Yb,n=2;Ln=Sm,Eu,Dy,n=1〕.All the water molecules were uncoordinated.Dinuclear complexes were observed in the coordination environment.The coordination number of central ions was nine.
经元素分析、红外光谱、紫外光谱、核磁共振谱、质谱、摩尔电导、差热热重分析确证结构，其化学式为C34H32O8N2LnCl·nH2O，简写为：(L42LnCl·nH2O，Ln=Nd，n=4；Ln=Pr，Yb，n=2；Ln=Sm，Eu，Dy，n=1；该类配体是以酚氧原子、亚氨基的氮原子、桥联的羧基氧原子以及氯原子同稀土离子配位，形成了九配位的双核配合物。
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In the third chapter, eight new complexes of 4, 6-dimethylpyrimidine 2-thioacetic acid with rare earth metals has been synthesized and characterized by means of elemental analysis, molar conductivity, IR,〓 NMR and TG-DTA. The general formula of the complexes is Ln〓(n=4 or 5). In the complexes, the deprotonated ligand coordinated to the rare earth metal ions in chelate bidentate mode. 4 or 5 molecular of crystal water existed in the complexes.
第三章合成了八种4，6-二甲基嘧啶-2-硫代乙酸的稀土配合物，通过元素分析、摩尔电导、红外光谱、核磁共振氢谱和热重-差热对配合物进行了表征，研究结果表明，配合物的组成为Ln〓n=4或5），在配合物中配体羧基脱去质子后采用螯合双齿的方式与稀土离子形成配位键，同时，配合物中含有4或5个结晶水。
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Two coordination polymers [Pb6(H2O)24]·3H2O(1)(H3cit=citric acid)and Pb(H2O)2(2)(tar=tartaric acid)were synthesized under hydrothermal conditions and characterized via IR,TG-DTA,C,H,N elemental analysis,XRD and single crystal X-ray diffraction analysis.
在水热条件下，合成了2个含柔性配体柠檬酸和酒石酸的二价铅配位聚合物[Pb6(H2O)24]。3H2O(1)(H3cit=citricacid)及Pb(H2O)2(2)(tar=tartaricacid)。用红外光谱、差热-热重、元素分析、粉末X射线衍射及单晶X射线衍射等手段对化合物进行了表征。化合物1属三斜晶系，P1空间群，a=0.97053(19)nm，b=0.9764(2)nm，c=1.0955(2)nm，α=109.016(3)°，β=98.380(3)°，γ=92.136(3)°，V=0.9671(3)nm3，Z=2，R1=0.0420，wR2=0.1049，GOF=1.064。
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thermal halogenation：热卤化作用
l grease cup 热脂杯 | thermal halogenation 热卤化作用 | thermal head 热能头,热位差