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The appropriate temperature of diazotization was-10～-5℃,and the diazotizating fluoborate was decomposed in petroleum ether to get 2-chloro-3-fluoropyridine with 64% yield.
以2-氯-3-氨基吡啶为原料，在40%的氟硼酸溶液中，采用饱和的亚硝酸钠为重氮化剂，在-10~-5℃下进行重氮化反应制得重氮盐，在石油醚中热分解得到2-氯-3-氟吡啶，收率为64%。
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When other factors are finable, 15L/h is the suitable amount of aeration.By analysis, the excessive aeration amount will destroy the capacity of sludge, and so decrease the removal efficiency of CODCr,and the 15L/h aeration amount is enouge for the demand of nitrification.
4蛭石应用于一级生物强化处理中，蛭石填料对有机物去除没有明显效果，但可以增加系统对氨氮去除能力，与对照组相比，高出30％多；吸附饱和后的蛭石，在活性污泥再生过程中，通过活性污泥的降解有机物，可去除较大部分的氨氮。
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Two technology including nitrocarburizing process and salt nitrocarburzing process haver been adopted. Several conclusions were obtained: firstly, nitrided layers consist of two layers including the outer white layer, mainly ε and γ′ with favorite errosion resistance, the inner dark layer consist of α-Fe.
再往里为扩散层，扩散层与原始组织无明显区别，是过饱和含氮的α-Fe固溶体，比原始组织更易受腐蚀；(2)试样经长时间氮碳共渗后，渗层最表面会出现疏松，这是因为Fe原子向外扩散，在ε相内造成Fe原子空位，空位向内扩散，并可能在晶界上或某些晶体缺陷处堆积，以致造成空洞。
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The results showed that: the influence of the aquaculture process on aquaculture water determined by type of aquaculture; the influence of aquaculture process on the water temperature, salinity and pH value were not wide.the descent of pH value was related to feed coefficients ; the dissolve oxygen of water in outfall was lower than the water in infall,but the concentration still maintained at the saturation level, is mainly affected by density of aquaculture ,rate of feed and artificial measures of increasing oxygen ;the major form of inorganic nitrogen was nitrate-N;the concentration of inorganic nitrogen and the organic matter tended to increase ,but the ammonium to decline ,this was relation with density of aquaculture ,rate of feed and variation of the different inorganic nitrogen form ; concentration of phosphate-P was low in outfall of pond , related with phosphate-P precipitating, as flowing water speed slowly in outfall;This phenomenon that the total number of bacteria and coli form group of water in outfall was lower than the water in infall , this caused by measures of sterilization and disinfection .
结果表明：养殖过程对水体影响与养殖类型有关。养殖过程对水体的水温、盐度和pH影响不大； pH下降与饲料系数高有关；溶解氧含量排水口比进水口低，但仍维持在饱和状态，与养殖密度、投饵率和人工增氧有关。硝酸氮是无机氮的主要存在形式，无机氮和有机物含量有升高趋势，氨氮有下降的趋势，与养殖密度，投饵率和各种无机氮之间的相互转换有关。活性磷酸盐含量在排水口含量下降，与排水口流水速度慢，磷酸盐沉淀有关。生物指标细菌总数和大肠杆菌总数在排水口比进水口低现象普遍存在，这与养殖场杀菌消毒等措施有关。
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With the increase of nitrogen dose, the amount of AIN increased, and the degree of saturation increased too, so the lattice constant of implanted layer increased.
随氮注入剂量的增加，AIN析出相的数量增加，铝合金中氮的过饱和程度增加，因此材料表层的点阵参数增加。
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In order to determine the saturated vapor pressure of colloid ed dinitrogen tetroxide,and find out its change rule with the various temperature,a testing equipment of determining satuated vapor pressure of colloid ed dinitrogen tetroxide was designed and constructed according to the principle of static testing.
为了测定胶体四氧化二氮的饱和蒸气压，找出其在不同温度条件下的变化规律，采用静态法测试原理，自行设计建立了四氧化二氮胶体饱和蒸气压的测试装置，测得了常压下液体和胶体四氧化二氮的饱和蒸气压数据，结果表明，四氧化二氮体系成胶后比成胶前的饱和蒸气压略有降低，且温度越高其差值越大。
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The invention concerns a process for preparing heterocyclic carbenes of general formula in which R1, R2, R3 and R4 are identical or different and mean saturated or unsaturated, straight-chain, branched or cyclic, unsubstituted or substituted C1-C10 alkyl, C2-C5 alkylidene, C2-C5 alkylidine, C7-C19 aralkyl or C6-C14 alkyl groups, R3 and R4 can also stand for hydrogen or form jointly anellated, substituted or unsubstituted groups with between 3 and 7 carbon atoms and X stands for carbon or nitrogen, R3 being dropped if X is nitrogen.
本发明涉及一种制备通式Ⅰ的杂环碳烯的方法，其中在通式Ⅰ中，R1、R2、R3和R4是相同的或不同的，并且是饱和的或不饱和的，直链、支链或环状的，未取代或取代的C1－C10－烷基、C2－C5－亚烷基、C2－C5－次烷基、C7－C19－芳烷基或C6－C14－芳基基团，R3和R4可以是氢或它们一起形成具有3－7个碳原子的稠合的、取代或未取代的基团，X是碳或氮，并且当X是氮时，不存在R3。
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The influence of organic loading, hydraulic loading, the ratio of gas and water and the height of filling to removal efficiency of COD, ammonic nitrogen and total nitrogen has been studied in BAF by using the self-confected wastewater.
中文摘要：本文以自配生活污水为实验用水，研究了有机负荷、水力负荷、气水比以及填料高度对BAF去除COD、氨氮、总氮的影响，并在沸石吸附饱和后对其进行生物再生。
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Synthesis of organic sulfuric compounds in aqueous media is carried out by: using thio-olefin compounds with carbonyl compounds, acetal/keltone, hydrazone, oxime, osazone and enamine to synthesize mercaptal/keltone compounds in aqueous media; using thio-olefin compounds with alpha-hydroxyaldehyde/keltone or alpha-halogenated aldehyde/keltone to synthesize thia-olefin derivatives in a queous media; using thio-olefin compounds with alpha, beta-unsaturated hydroxy compounds, C-C treble bond, C-N treble bond, C-C double bond, N-N double bond, C-N double bond, C-S double bond, epoxy and its derivatives, aziridine and its derivatives, cyclopropane and its derivatives and halogenated carboxy to synthesize sulfoether compounds in a queous media.
含水介质中有机硫化合物的合成方法，本发明属于有机合成方法，用硫缩烯酮类化合物与羰基化合物、缩醛/酮、腙、肟、脎、烯胺在含水介质中合成缩硫醛/酮化合物，与α-羟基醛/酮或α-卤代醛/酮在含水介质中合成噻烯类衍生物，与α，β-不饱和羰基化合物、碳碳叁键、碳氮叁键、碳碳双键、氮氮双键、碳氮双键、碳硫双键、环氧乙烷及其衍生物、氮杂环丙烷及其衍生物、环丙烷及其衍生物、卤代烃等在含水介质，中合成硫醚化合物。
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The adsorption of NH〓 in the 〓CO〓 solution and the adsorption of NH〓-N in the waste water from the Coking plant,Capital Iron and Steel Coripo ration by bentonite were investigated. The results show that the amount of 〓 adsorbed by particulate betonite (〓1. 68mm) and -200 mesh bentonite are 26. 39 and 8. 87mg/g, respectively; and the amount of NH〓-N in the waste water from the coking plant adsoybed by particulate bentonite, acid activated bentonite and -200 mesh bentonite are 32. 00, 21. 85 and 15. 62mg/g, respectively.
对膨润土吸附溶液中的 NH〓离子和从首钢公司焦化厂焦化废水中去除氨氮进行的试验研究结果表明，该膨润土对碳酸铵溶液中 HN〓离子的饱和吸附量是颗粒膨润土26.39mg/g、粉状膨润土8.87mg/g；对焦化废水中氨氮的饱和吸附量是颗粒膨润土32.00mg/g、活性膨润土21.85mg/g和粉状膨润土15.62mg/g。
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Tissue Halftime：半饱和组织时间
余氮排除总时间 Residual Nitrogen Time | 半饱和组织时间 Tissue Halftime | 潜水后可飞行所需时间 Flying After Diving Time
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nitrify：用氮饱和
nitrify 使与氮化合 | nitrify 用氮饱和 | nitrifying 硝化的
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nitrify：使与氮化合
nitrifier 硝化细菌 | nitrify 使与氮化合 | nitrify 用氮饱和
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trisazo：三偶氮的
trisaturatedglyceride 三饱和酸甘油酯 | trisazo 三偶氮的 | trisazocompound 三偶氮化合物
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nitrifying：硝化的
nitrify 用氮饱和 | nitrifying 硝化的 | nitrile 腈