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A series of p-toluene sulfonylamido acetacylhydrazone derivatives were synthesized from p-toluenesulfonyl chloride which reacted with glycine to get the intermediate p-toluene sulfonylamido glycine, then through the esterification, hydrazinolysis to afford another intermediate p-toluene sulfonylamido acethydrazide, which condensed with different aldehydes to obtain the target compounds that were characterized by IR, 1H NMR, 13C NMR spectra and elemental analysis.
魏太保 ；冷艳丽；王永成；张建辉；张有明*摘要：以对甲苯磺酰氯为原料，通过与氨基乙酸反应得到中间体对甲苯磺酰氨基乙酸，再经酯化、肼解得到对甲苯磺酰氨基乙酰肼，然后与相应的醛缩合得一系列对甲苯磺酰胺基乙酰腙类化合物。其结构经元素分析， IR， 1H NMR和13C NMR确证。
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The condensation of 3 carbethoxy isoquinol 4 one with carbamidine, amidine, carbamide and sulfocarbamide gave isoquinolo pyrimidine derivatives, respectively and isoquinolo quinoline derivatives were synthesized by the reaction of o aminobenzaldehyde or o aminopiperonal with isoquinol 4 one.
报道了利用 3 乙氧甲酰基异喹啉 4 酮分别与胍、脒、脲及硫脲类化合物缩合反应合成异喹啉并嘧啶衍生物，邻氨基苯甲醛、邻氨基胡椒醛分别与异喹啉 4 酮反应合成异喹啉并喹啉化合物。6个新化合物的结构通过元素分析、红外光谱、核磁共振氢谱和质谱予以证
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Carbamide reacting with H2SO4 forms aminosulfonic acid. Allantoin is prepared by oxidation of the aqueous solution of glyoxal into glyoxylic acid which is then used to synthesize allantoin.
氨基磺酸的合成是用尿素和发烟硫酸反应；尿囊素的合成是用硝酸氧化乙二醛溶液制得乙醛酸后，再加入氢氧化钙和氯化钙，使乙醛酸以钙盐形式析出，然后在盐酸介质中与尿素缩合而成。
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The o-aminobenzaldehyde ethylene acetals can be synthesized from corresponding o-nitrobenzaldehyde by reducing the nitro-group after the protection of carbonyl by ethylene. 2-Aminophenyl ketone ethylene ketal can also be prepared from 2-nitrophenyl ketones by this method.
邻氨基苯甲醛乙二醇缩醛可以由含不同取代基的邻硝基苯甲醛经羰基以乙二醇缩醛保护后还原硝基得到，邻氨基芳香酮乙二醇缩酮可以同样的方法由邻硝基芳香酮得到。
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The intermediate 5-amino-1H-pyrazole-4-carboxylic acid ethyl ester prepared in the first part underwent successively hydrazinolysis, condensations with ketene dithioacetals and alkylations to give rise to the dipyrazolyhnethanes.
从第一部分中的中间体5-氨基-1H-吡唑-4-羧酸乙酯开始，经过肼解、与乙烯酮二硫代缩醛的缩合反应和烷基化反应，合成了二吡唑基甲酮类化合物。
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aminoacetal：氨基乙缩醛
amino 氨基的 | aminoacetal 氨基乙缩醛 | aminoacyl 氨基酰