- 更多网络例句与氟化氧相关的网络例句 [注:此内容来源于网络,仅供参考]
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Nucleophilic opening of the terminalepoxide 57 by a lithium acetylide from 27 in the presence of BF3·EtO furnishedcompound 58, which had the skeleton of target molecule, subsequent conversionsinvolved the introduction of γlactone gave Annonacin.
然后以三氟化硼参与的炔负离子开环氧反应建立分子骨架,得到化合物58。随后经氢化,引入α,β不饱和丁内酯环、去保护等几步反应,就得到Annonacin。
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In this research, we used a sol-gel process to prepare UV-curable antiglare coatings. First the inorganic monomer tetraethoxylsilane was formed into colloidal silica by hydrolysis and condensation reactions. Then, added the couple agent 3- propyl methacrylate and surfactant fluoroalkylsilane (13F) to modify the colloidal silica. Finally, organic monomer dipentaerythritol hexaacrylate were added to form hybrid material.
中文摘要本研究是经由溶胶凝胶制程,将无机单体四乙氧基矽烷先行水解、缩合反应成为二氧化矽,接著分别加入偶合剂三异丙基矽基丙烯酸酯、氟化矽氧烷(13F)、对二氧化矽微粒进行表面改质;之后再导入交联剂DPHA加以强化合成出奈米混成涂料。
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The 3-chloro-4-trifluoromethoxy benzonitrile was synthesized from 3-chloro-4-trifluorome- thoxy aniline by diazotization, formaldoximation ,hydrolysis and cyanation.
以3-氯-4-三氟甲氧基苯胺为原料,经重氮化、甲醛肟化、水解和腈化反应得到纯度≥99。
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The crosslinked PEG-20M glass capillary column was prepared by dynamic coating method with boron trifluoride as catalyst,3-glvcidyl-oxypropyl-trimethoxysilane as crosslinking agent.
以PEG-20M为固定相,三氟化硼为催化剂,3-缩甘油氧丙基三甲氧基硅烷(简称KH-560)为交联剂,二氯甲烷为溶剂,对预先用氯化钠沉积法粗糙化的玻璃毛细管柱进行动态涂渍。
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Nitratomethyl-3-ethyloxetane was synthesized by the process of cyclization, nitation from trimethlolpropane and diethyl carbonate, and the homopolymer of 3-nitratomethyl-3-ethyloxetane was synthesized with 1,4-butanediol as initator and boron trifluoride etherate as an catalyst by cationic ring-opening polymerization.
以三羟-甲基丙烷和碳酸二乙酯为原料经环化、硝化两步反应合成了化合物3-硝酸酯甲基-3-乙基氧丁环;采用1,4-丁二醇为引发剂,三氟化硼乙醚(BF3Et2O)为催化剂,NIMEO发生阳离子开环聚合得到一种端羟硝酸酯均聚醚PNIMEO。
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Using butanediol as initiator, boron-trifluoride etherate as catalyst, 3-azidomethyl-3-methyloxetane homopolymer was synthesized by the cationic polymerization of 3-azidomethyl-3-methyloxetane which was carried out in dichlorometane.
以1,4-丁二醇为引发剂,以三氟化硼乙醚络合物为催化剂,以3-叠氮甲基-3-甲基氧丁环为单体,以CH2Cl2为溶剂,按阳离子开环聚合机理,合成了含能粘合剂3-叠氮甲基-3-甲基氧丁环均聚物。
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Using pentaerythritol as initiator, boron trifluoride diethyl etherate as catalyst.dichloroethane as dispersion agent, the chloride polyether polyol is synthesized based on the mechanism of cationic ring-opening polymerization of epiclilnrohyclrin.The azide polyether polyol is synthesized, in DMF through A and sodium azide, and the non-reported azide energetic curing agent is synthesized through the adduction of B and IIDI.
以季戊四醇为起始剂,三氟化硼乙醚为催化剂,1,2—二氯乙烷为分散剂,环氧氯丙烷经阳离子开环聚合反应制成氯化聚醚多元醇,A在N,N—二甲基甲酰胺中与叠氮化钠反应制得叠氮聚醚多元醇,B与六亚甲基二异氰酸酯加成反应制得未见文献报道的叠氮固化剂。
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Water samples were extracted and purified and collected by solid-phase extraction LC-18 column. Soil samples were extracted by ethyl acetate/petroleum ether (2:1, by vol) and purified by sulphonation. Wheat sample was extracted by acetonitrile/water (4:1, by vol) and purified and collected by SPE- Florisil column.
水样直接用LC-18固相萃取小柱分离、净化和富集;采用乙酸乙酯/石油醚(体积比2:1)振荡提取,磺化法净化,测定土壤中氯氟吡氧乙酸残留量;以乙腈/水(体积比4:1)为提取剂,氟罗里硅土固相萃取小柱分离、净化,测定小麦样品中氯氟吡氧乙酸的残留量。
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It reacts violently with oxygen difluoride and barium peroxide.
一氧化碳同氟化氧、氧化钡会发生剧烈反应。
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Optimum conditions are as follows: DMF is used as solvent, compound quaternary ammonium salt as catalyst, n(p-nitrochloro benzene):n=1: 1.2, m:m(p-nitrochloro benzene)=4%, m:m(p-nitrochloro benzene)1:1, and reacted under 155~160℃ for 18 h; reduction reaction is carried out in methanol with Raney nickel, which is used as catalyst; the raw product is added an antioxidant, and distilled simply under reduced pressure to obtain 4-fluoroaniline with excellence quality, purity is over 99.5%, total yield is 89.3%.
实验结果表明,氟化反应的最佳条件为:二甲基甲酰胺为溶剂、复合季铵盐为催化剂,n:n=1:1.2,m(催化剂:m=4%,m:m=1:1,于155~160℃下反应18h;还原反应在甲醇中进行,以阮内镍为催化剂;粗产品加入抗氧剂,减压条件下简单蒸馏得高品位的对氟苯胺。
- 更多网络解释与氟化氧相关的网络解释 [注:此内容来源于网络,仅供参考]
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sulfuryl fluoride:氟化硫醯
Sulfuric Acid 硫酸 | Sulfuryl Fluoride 氟化硫酰 | Tantalum Pentoxide 五氧化二钽
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bismuthyl fluoride:氟化氧铋
bismuthyl dichromate | 重铬酸氧铋 | bismuthyl fluoride | 氟化氧铋 | bismuthyl hydroxide | 氢氧化氧铋
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bismuthyl hydroxide:氢氧化氧铋
bismuthyl fluoride | 氟化氧铋 | bismuthyl hydroxide | 氢氧化氧铋 | bismuthyl | 氧铋基
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bismuthyl dichromate:重铬酸氧铋
bismuthyl chloride | 氯化氧铋 | bismuthyl dichromate | 重铬酸氧铋 | bismuthyl fluoride | 氟化氧铋
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chloryl fluoride:氟化氯氧
Chlorvalamide | 杀草利 | chloryl fluoride | 氟化氯氧 | chlorylene | 三氯乙烯
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oxyfluoride:氟化氧
oxycodone 氧可酮 | oxyfluoride 氟化氧 | oxygen-poor 缺氧
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carbon oxyfluoride:氧氟化碳
一氧化碳 carbon monoxide | 氧氟化碳 carbon oxyfluoride | 氧硫化碳 carbon oxysulphide
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bismuth oxyfluoride:氟氧化铋 氟化氧铋
bismuth oxybromide | 溴氧化铋 | bismuth oxyfluoride | 氟氧化铋 氟化氧铋 | bismuth oxyiodide | 碘氧化铋
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platinous hydroxide:氢氧化铂(II);二(氢氧)化铂
氟化铂(II);二氟化铂 platinous fluoride | 氢氧化铂(II);二(氢氧)化铂 platinous hydroxide | 碘化铂(II);二碘化铂 platinous iodide
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vanadous fluoride:三氟化钒
vanadous chloride 二氯化钒 | vanadous fluoride 三氟化钒 | vanadyl chloride 氯化氧钒