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Results of test showed that DFA-PEG polyester and its derivant had excellentemulsification performance, and emulsion was exquisite and steady, the surfacetension and critical micelle concentration of DFA-PEG polyester and sulfatedDFA-PEG polyester were very low, DFA-PEG polyester terminated with rosin acid hadcertain antifoaming performance, but surface tension and CMC increase to extent.
性能测试表明，DFA-PEG聚酯及其两种衍生物均具有优良的乳化性能，乳液细腻且稳定；DFA-PEG聚酯及其硫酸酯盐水溶液的表面张力和临界胶束浓度较低：DFA-PEG聚酯松香酸酯还具有一定的抑泡性能，与DFA-PEG聚酯及其硫酸酯盐比，其水溶液表面张力和临界胶束浓度有所增加。
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DFA-PEG polyester was synthesized with DFA and PEG 400 at first, and then bysulfating DFA-PEG polyester with NH_2SO_3H or terminating DFA-EG polyester withrosin acid, two derivant, these are sulfated DFA-PEG polyester and terminateDFA-PEG polyester, were synthesized. The reaction conditions of synthesis wereoptimized by orthogonal experiments.The molecular weight of product was analyzed by GPC.
5以二聚脂肪酸和聚乙二醇400为原料，首先合成了DFA-PEG聚酯，再以DFA-PEG聚酯为衍生体，硫酸化或用松香封端，合成了两种DFA-PEG聚酯衍生物——DFA-PEG聚酯硫酸酯盐和松香酸封端DFA-PEG聚酯，通过正交试验，对合成的条件进行了优化。
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In this paper, firstly using natural fatty acids including lauric acid, myristic acid, palmitic acid etc. and disproportionated rosin as starting materials, the acyl reaction of starting materials with SOCl_2 respectively, and then using Schotten-Baumann condensation: on the reaction conditions of alkalescence, condensation of acylchloride with amino acid (sarcosine, glycine, alanine etc.), and then acidification, saltation. A series of anionic surfactants of N-acyl amino: sodium N-fatty acyl sarcosinate (SFS-12, SFS-14, SFS-16); sodiun N-fatty acyl glycinate(SFG-12, SFG-14, SFG-16); sodium N-fatty acyl alaninate(SFA-12, SFA-14, SFA-16)and sodium N-disproportionated rosinoyl aminatewere prepared. During the preparation of N-acylamino acid, the reaction conditions of acylchloride with amino acid condensation were identified by optimizing the synthetic conditions of N-lauroyl sarcosine: mol ratio of amino acid to acylchloride 2:1, reaction taken place in a solvent composed by acetone/water 2:1, acylchloride and 20% NaOH were slowly added to the reaction mixture at the same time while maintaining the pH at 9~10, after completion of adding maintaining reacting for 2.5h at 25℃.
首先以月桂酸、肉豆蔻酸、棕榈酸等天然脂肪酸和歧化松香为原料，与氯化亚砜反应制得酰氯，然后采用Schotten-Baumann 缩合法路线，即在碱性条件下，酰氯和氨基酸(肌氨酸、甘氨酸、丙氨酸等)缩合，经过酸化、成盐，合成一系列氨基酸型阴离子表面活性剂：脂肪酰肌氨酸钠，即月桂酰肌氨酸钠(SFS-12)、肉豆蔻酰肌氨酸钠(SFS-14)、棕榈酰肌氨酸钠(SFS-16)；脂肪酰甘氨酸钠，即月桂酰甘氨酸钠(SFG-12)、肉豆蔻酰甘氨酸钠(SFG-14)、棕榈酰甘氨酸钠(SFG-16)；脂肪酰丙氨酸钠，即月桂酰丙氨酸钠(SFA-12)、肉豆蔻酰丙氨酸钠(SFA-14)、棕榈酰丙氨酸钠(SFA-16)；N-歧化松香酰基氨基酸钠(sodium N-disproportionated rosinoyl aminate)，即N-歧化松香酰基肌氨酸钠(sodium N-disproportionated rosinoyl sarcosinate ，简称SDRS)、N-歧化松香酰基甘氨酸钠(sodium N-disproportionated rosinoyl glycinate，简称SDRG)、N-歧化松香酰基丙氨酸钠(sodium N-disproportionated rosinoyl alaninate，简称SDRA)。
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To study the relationship between the "tail" structure and the characteristics of Gemini surfactants, a new gemini surfactant CH(subscript 2s)-αω-Bis (dehydroabietyihydroxypropyltetramethylethyldiammonium Chloride) here s=2, has been synthesized. Dehydrogenated rosin as hydrophobic "tails" in the structure. The affections of reacttants ratio, reaction temperature and time on the yield of aimed compound have been discussed.
研究了Gemini表面活性剂中疏水&尾巴&结构对性质的影响，以脱氢松香酸和环氧氯丙烷为原料合成了中间体3-脱氢松香酰氧－2-羟丙基氯，再与四甲基乙二胺反应，得到1种以脱氢松香酰基为疏水链&尾巴&的对称Gemini型双季铵盐阳离子表面活性剂：二氯化－N，N'-二（3-脱氢松香酰氧－2-羟丙基）四甲基乙二胺。
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To study the relationship between the hydrophobic "tail" structure and thecharacterizations of Gemini surfactants, a new gemini surfactant CsH2s-α,ω-bis(dehydroabietylhydroxypropylteteramethylethylammonium Chloride),here s=2, wassynthesized. Dehydrogenated rosin as hydrophobic "tails" in the structure. The impact factorsin the two steps are discussed.
为研究gemini表面活性剂中疏水&尾巴&结构对性质的影响，本论文以脱氢松香酸和环氧氯丙烷为原料合成了中间体3-脱氢松香酰氧-2-羟丙基氯，再与四甲基乙二胺反应，得到一种以脱氢松香酰基为疏水链&尾巴&的对称gemini型双季铵盐阳离子表面活性剂：二氯化-N，N′-二(3-脱氢松香酰氧-2-羟丙基)四甲基乙二胺。
- 更多网络解释与松香酸盐相关的网络解释 [注：此内容来源于网络，仅供参考]
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maleate：马来酸盐 马来酸盐酯 马来酸酯 顺丁烯二醛
maleass 雄驴 | maleate 马来酸盐 马来酸盐酯 马来酸酯 顺丁烯二醛 | maleatedrosin 马来松香
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sima sphere：硅镁带
silvinate 松香酸盐 | sima sphere 硅镁带 | sima 硅镁圈
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abies oil：松针油
Abel-Pensky closed tester阿贝尔-宾斯基密闭式闪点试验器 | abies oil 松针油 | abietate 松香酸酯;松香酸盐
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abietate：松香酸酯;松香酸盐
abies oil 松针油 | abietate 松香酸酯;松香酸盐 | abietene 松香烯
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abietene：[化] 枞烯; 松香烯; [医] 松香烯
1536abietate[医] 松香酸盐 | 1537abietene[化] 枞烯; 松香烯; [医] 松香烯 | 1538abietic[医] 松香的
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sylvate：松香酸盐
sylvanite 针碲金矿 | sylvate 松香酸盐 | sylvatron 电光管
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diazotized compound：重氮化合物
diazotization 重氮化(作用) | diazotized compound 重氮化合物 | dibasic aluminum monorosinate 单松香酸铝二代盐
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pink salt：锡盐
pinic acid 蒎酸 | pink salt 锡盐 | pinoline 松香烃