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In this thesis,the authors analyze the mechanism of roadway roof absciss layer ,point out the demerits of traditional methods of measuring roadway roof absciss layer , treatise the principles and put forward some methods of measuring absciss layer by minging vibration method.
分析了巷道顶板离层的机理,指出了传统测量离层方法的弊端,论述了采矿振动法测量离层的原理,提出了采矿振动法测量离层的方法。
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The exact of petroleum ether was the acaricidal active site of Eungenia caryophyllata. 3.Isolation, purification and identification of compounds with acaricidal activity in Eugenia Caryphyllata: The exact of petroleum ether was separated into 6 parts by silica gel column chromatography with gradually increasing polarity of petroleum ether: ethyl acetate. The part C was demonstrated to be the most effective part by acaricidal activity test in vitro,and the time for it to kill all experimental mites was about 20 min.
丁香杀螨活性成分的追踪分离、纯化与结构鉴定:采用硅胶柱层析法,以石油醚:乙酸乙酯溶剂系统梯度洗脱,对丁香石油醚提取物进行分离,得到A~F 等6 段混合物,离体杀螨试验发现,C 段混合物具有突出的杀螨活性,50%浓度平均15min可杀死全部供试螨虫。
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It is a organic hexahydric weak acid. In different acidity, the dissociation degree and the color of reagent solvent were different also. Determined and draw the absorption curve of reagent in varies acidity, and figured out the dissociation constant by Perisic-Janjic method; the complex ratio of the reagent and bismuth was determinated by mole ratio method and continuous variation method; The apparent stability constant of the complex was calculated, the mechanism of dissociation and coordination were discussed.
2,6—二溴4—硝基偶氮氟胂是本实验室合成的测定铋的一个较好的试剂,对其进行了进一步的研究,在用柱层析法对其进行了提纯后,测定了试剂在不同酸华东师范大学硕:l:学位论文摘要度下的吸光度和最大吸收波长,绘制了其吸收曲线,用Perisic一Janjic法计算了试剂的六级离解常数;用摩尔比法和连续变化法测定了试剂与秘形成的配合物的络合比:计算了配合物的表观稳定常数,研究了其离解和配合机理,为筛选高效有机显色剂提供了理论依据。
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Six experimental stages were designed in our procedure, those are:(1) metabolite recovery and tested sample preparation: the metabolites were recovered by Amberlite XAD-2 absorption, followed by MeOH elution and solvent concentration;(2) antioxidant detection and strain selection: samples were quantitatively analyzed by the inhibition effects on formation of lipid peroxides and TBARS to screen the strains able to produce antioxidants. According to the established screening methods, we chose out a strain of actinomycetes, designed as AMBL-029C;(3) antioxidant purification: the fermentation broth was recovered by a series of separation techniques including centrifugation, Amberlite XAD-2 absorption, followed by MeOH elution and a successive TLC purification. The resulting primary purified compound [temperately designed as AMBL-029C-TS] was further analyzed by HPLC to monitor its purity;(4) physical-chemical characteristics: judging from the acid-base fractionation experiments, and the pH and temperature stability tests, the compound was deduced to be a acidic compound with the properties of low polarity and highly pH and temperature stable;(5) mechanism of the antioxidant: in comparison with some other known antioxidants, TS was subjected to investigate its antioxidant mechanism, together with BHT,-tocopherol, as well as two streptomyces metabolites, homogentisic acid and -phenylpyruvic acid, which were previously isolated as the natural antioxidants in our laboratory.
针对本实验目的,我们设计了以下的实验步骤﹔(1)二次代谢物回收及检测样本处理:我们将发酵所得的培养上清液,利用疏水吸附性树酯Amberlite XAD-2吸附回收,并以甲醇溶离及真空减压浓缩脱水等方式处理,以取得提供抗氧化活性筛选之检测样本;(2)抗氧化活性检测及菌种筛选:以「过氧化脂质」和「硫丙二醯尿」的生成量进行定性定量分析以作为抗氧化物质生产菌筛选之用;经此筛选程序,我们选获了具有抗氧化物质高生产力的菌株,命名为AMBL-029C;(3)抗氧化物质的分离纯化:针对生产菌株的发酵回收处理液,以矽胶薄层色层分离法经物质层析纯化后,并以高效能液相层析法(High performance liquid chromatography;HPLC)分析物质可得一初级纯化物质,命名为AMBL-029C-TS;(4)抗氧化物质的物理化学性质分析:由酸碱转溶(acid-base fractionation)实验得知,此抗氧化物质属於中低极性的强酸性物质,对温度(37℃-100℃)及酸碱度(pH3.0-13.0)均表现出高稳定性;(5)在抗氧化机制探讨方面,我们针对数种不同的抗氧化机制进行探讨,即: 1。
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In order to discuss the effect of overburdens under injecting grouts in separate layers on the morphology of the water flowing fractured zone, continuous exploration for failure characteristics of the overburden of working face 14308 of Dongtan Coal Mine under injecting grouts in separate layers and fully mechanized sub-level caving condition was processed by the method of underground uphole water injection technology by intervals with bore-head leaking multi-loops affusion system.
为了探讨覆岩离层注浆条件对导水裂隙带形态的影响,采用前端泄露式多回路注水系统,应用井下仰孔分段注水法对东滩煤矿14308工作面覆岩离层带实施注浆充填条件下综采放顶煤导水裂隙带的破坏特征进行了连续探测。
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The lagging is terminated 75mm either side of each flange joint and separate lagging with removable aluminium covers are used over the flanges.
保温层离两端法兰各 75mm,分开的保温层及法兰都用可动的铝蒙皮覆盖住。
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Citric Acid:檬酸
本法是用拧檬酸 (Citric acid) 与珍珠粉、层粉及贝壳粉等作用,生成柠檬酸钙等可溶性柠檬酸盐. 目前在英、美等国际市场上以采用拧檬酸盐法为多,由于此法生成的盐类水解度较高,生理宽容性大,被离解的酸根亦可被人体内直接吸收代谢,
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chromatography:层析法
[目录] 基本知识 特点 基本原理 层析分类 [原文] 基本知识 层析法(Chromatography)又称色谱法、色层法或层离法,是目前广泛应用的分离技术. 层析法是利用不同物质的某些理化性质的差异而建立起来的技术. 组成 固定相
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chromatographic:色析法的, 层离法的
chromatographic technique | 色谱技术 | chromatographic | 色析法的, 层离法的 | chromatographically | 色析法地, 层离法地
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normal abscission layer development of hilum:种脐的正常离层发育
normal abscission ==> 正常离层 | normal abscission layer development of hilum ==> 种脐的正常离层发育 | normal acceleration ==> 法向加速度