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Part 2. Annulation reaction of 3, 4-dichlorocoumarin (1) and 3, 4-dichloromaleimide (8) by a new general annulation strategy developed in this group with 2-phenylbenzofuran (15), 3-phenylbenzofuran (16), 2, 5-diphenyloxazole (17), 2, 5-diphenylthiazole (18), 2-methyl-4-phenylthiazole (19) and 2, 3-dimethoxy-1, 3-butadiene (40) were investigated.
二。在本课题组前一阶段提出的从二氯代环烯酮与1，1-二芳基乙烯的光化反应以及光化反应中得到的环丁烷产物的连续电环化反应对3，4-二氯马来酰亚胺以及3，4-二氯香豆素进行增环反应的工作基础上，研究了3，4-二氯香豆素（1）和3，4-二氯马来酰亚胺（8）与5个α-苯基取代的环烯烃2-苯基苯并呋喃（15），3-苯基苯并呋喃（16），2，5-二苯基噁唑（17），2，5-二苯基噻唑（18），2-甲基-4-苯基噻唑（19），以及一个丁二烯——2，3-二甲氧基丁二烯（40）进行的芳香族增环反应。
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They are 4-(2- hydroxy-3-butynlenoxy) benzoic acid (1, WA), 5-chloro-7, 8-dihydroxy-7-methyl- 6-oxo-3- [ -3, 4-dihydroxy-3, 5-dimethyl-l-heptylene] -1H-8, 8a-dihydrobenzo [2, 3-c] pyran (2, WB),-2-(2-methyl-2-dibutene diamido)-2-butenoic acid (3, B5262), 3, 4-dihydro-9, 10-dihydroxy-7-methoxy-3-methyl-1H-naphtho [2, 3- c] pyran-1-one (4, A73 semi-Vioxanthin), 8, 8'-bis (6, 9-dioxo-3,4-dihydro-10- hydroxy-7-methoxy-3-methyl-1H-naphtho [2, 3-c] pyran-1-one)(5, A122 Xanthomegnin), 2, 5-dioxo-3a-hydroxymethyl-3, 3a, 6, 6a-tetrahydro-furo [2, 3-b] furan (6, 1003-2), 7-acety1-5-chloro-6, 8-dioxo-7-methyl-3- [ -3, 5-dimethyl-1, 3- diheptylene] -4aH-benzo [2, 3-c] pyran (7, M2-2 sclerotiorin), respectively.
它们分别被命名为4-（2-羟基-3-丁炔氧基）苯甲酸（1，WA）、5-氯-7，8-二羟基-7-甲基-6-氧代-3-[-3，4-二羟基-3，5-二甲基-1-庚烯基]-1H-8，8a-二氢苯并[2，3-c]吡喃（2，WB）、-2-（2-甲基-2-丁烯二酰亚胺基）-2-丁烯酸（3，B5262）、3，4-氢-9，10-二羟基-7-甲氧基-3-甲基-1H-萘并［2，3-c］吡喃-1-酮（semi-Vioxanthin，4，A73）、8，8'-双（6，9-二氧代-3，4-二氢-10-羟基-7-甲氧基-3-甲基-1H-萘并［2，3-c］吡喃-1-酮）（Xanthomegnin，5，A122）、2，5-二氧代-3a-羟甲基-3，3a，6，6a-四氢-呋喃并［2，3-b］呋喃（6，1003-2），7-乙酰基-5-氯-6，8-二氧代-7-甲基-3-［-3，5-二甲基-1，3-庚二烯基］-4aH-苯并2，3-c］吡喃（Sclerotiorin，7，M2-2）。
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Results Twain-80 can increase the solubility. The dimethylsulfoxide, the sorbic acid and acetic acid chlorine can strengthen its bacteriostasis effect. To choice suitable antiseptic temperature and control antiseptic time may enhance furacilin liquid preparation stability. On the contrary, it may reduce the stability when mixing the antioxidants agents such as the sodium hyposulfite and the sodium bisulfite.
结果 吐温-80可增溶；二甲基亚砜、山梨酸和醋酸氯己定可增强其抑菌效果；选择适宜灭菌温度、控制灭菌时间可提高呋喃西林液体制剂的稳定性；加入硫代硫酸钠和亚硫酸氢钠做抗氧化剂则使其稳定性降低。
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Within this study, we found some interesting results, for example, the type of ring opening mode of methylene cyclopropyl ketones was changed from distal to proximal under the catalysis of palladium with the addition of two equivalents of sodium iodide.
我们发现了一个非常有趣的现象：亚甲基环丙烷基酮的开环方式可以得到有效的调控：在没有外加卤离子的情况下，开环方式为distal断裂，从而得到了4—氢吡喃化合物，而在两当量的碘化钠的存在下却发生了proximal断裂，从而能够得到2，4—双取代的呋喃。
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Chapter 1: The reactions of methylenecyclopropanes with phenylsulfenyl chloride or phenylselenyl chloride give cyclobutene derivatives along with ring-opened products in good total yields at 0 °C in various solvents. The reactions of methylenecyclopropanes with diphenyl diselenide give the di-phenylselenyl substituted ring-opening products which can be transformed to 2,5-dihydrofuran derivatives under the oxidation with hydrogen peroxide at room temperature.
在第一章中，我们发现亚甲基环丙烷类化合物在0℃时即可很快与苯硫氯或苯硒氯发生反应生成取代环丁烯类化合物和正常的开环产物；而与二苯基二硒的反应则需加热到150℃以上才能进行反应，生成的二苯硒基开环产物在双氧水氧化下可以转化为取代二氢呋喃类化合物。
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The chemical constituents of extracts of Tamarindus indica L were determined by GC-MS. The relative contents of constitutes were determined by area normalizing method. 48 compounds were identified, amounting to total mass fraction 98.5%. The main compounds were 5-methyl-2(3H)-furanone, diethyl succinate, furfural, hexadecanoic acid, linolenic acid, 5-methylfurfural, oleic acid, linoleic acid, etc.
并利用气相色谱仪-质谱仪对罗望子萃取物的化学组成进行了分析鉴定，并用面积归一化法测定了各种成分的质量分数，共鉴定了48种成分，占总质量分数为98.35%，其中主要成分为：5-甲基-2(3H)-呋喃酮、丁二酸二乙酯、糠醛、十六酸、亚麻酸、5-甲基糠醛、油酸、亚油酸等。
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Seauckthorn juice can be appropriate drinks afer the diluting, which could block the N-nitroso Synthesis and also can block N-dimethylnitrosaminewhich can lead to cancer.The flavone of Seabuckthorn contains coumarin, isocoumarin, furan coumarins, lignin, as well as bitter polyphenols, 5 - serotonin, which are benefited for anti-cancer.
沙棘汁经稀释成宜引用的浓度后，能阻断N-亚硝酸的合成，另外沙棘汁对致癌物N二甲基亚硝胺也有阻断与防护的作用；沙棘黄酮中含有香豆素，异香豆素，呋喃香豆素，苦木素以及多酚类，5-色胺等具有综合抗癌作用的成分。
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The stereochemical structures of two new compounds, 5-(3-chlorophenyl)-2-furfur-aldehyde-N-4-methylphenyloxyacetylhydrazone and 5-(3-chlorophenyl)-2-furfuraldehyde-N-4-nitrophenyloxyacetylhydrazone, were determined by DPFGSE-NOE experiments performed in DMSO-d\-6 at 25 ℃ and variable-temperature ~1H NMR The ~1H chemical shifts of the compounds were completely assigned at 25 ℃ and 90
利用变温实验和DPFGSE NOE实验，确定了 5 (3 氯苯基) 2 呋喃甲醛 N 4 甲基苯氧乙酰腙和5 (3 氯苯基) 2 呋喃甲醛 N 4 硝基苯氧乙酰腙两个新化合物25 ℃时在二甲基亚砜中的空间构型，并对这两个新化合物在 25 ℃和 90 ℃时的质子的化学位移进行了全归属。
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华派公司产品：对氯苯酚，邻氯苯酚，2，4二氯苯酚，2，6二氯苯酚，2，4，5三氯苯酚，2，4，6三氯苯酚，4氯2苄基苯酚，对溴苯酚，2，4，6三溴苯酚，对氯苯基叔丁基醚，间溴苯甲醚，间溴氟苯，α溴甲基四氢呋喃，α溴代4氯苯乙酮，α溴4甲氧基苯乙酮，4氯二苯甲酮，4氯2甲基苯胺，N(2羟乙基)乙二胺， 2，3二溴丙酰氯，对溴苯磺酰氯，对苯二甲酰氯，间苯二甲酰氯，N氯代丁二酰亚胺，N溴代丁二酰亚胺，四氯苯醌，5氯靛红。
- 更多网络解释与呋喃亚甲基相关的网络解释 [注：此内容来源于网络，仅供参考]
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PEI：聚醚酰亚胺
03) 聚醚酰亚胺(PEI)材料的分类体系D5315-04 用伴有支柱衍生作用的直接注水高压液相色谱法(HPLC)法测定水中N-甲基-氨基甲酰肟和N-氨基甲酸甲酯的试验方法D5341-99(2004) 测量焦炭活性指数(CRI)和反应后的焦碳强度(CSR)的试验方法D5376-93(2002) 橡胶的化学试验方法.测定橡胶防老化剂中氮的百分比含量:聚合的四氢呋喃(TMQ)D5
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benzothiofuran; benzothiophene; thianaphthene; thionaphthene：苯并硫呋喃;苯并噻吩;噻[口+奈]
苯甲酰磺酰亚胺;糖精;沙卡林 benzosulfimide; s... | 苯并硫呋喃;苯并噻吩;噻[口+奈] benzothiofuran; benzothiophene; thianaphthene; thionaphthene | 三氯甲基苯;次苄氯 benzotrichloride; benzotrichloride; benz...
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fural：呋喃亚甲基
furadantin呋喃丹啶 呋喃妥因 | fural呋喃亚甲基 | furaldehyde呋喃甲醛
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furfurylidene：呋喃亚甲基;亚糠基
呋咕基;呋吖基 furazanyl | 2-呋喃亚甲基;亚糠基 furfurylidene | 呋喃基 furyl
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furyl：呋喃基
2-呋喃亚甲基;亚糠基 furfurylidene | 呋喃基 furyl | 亚二氢呋喃基 furylidene