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The common chemical constituents were juniper camphor,1,3,3-trimethylcyclohex-1-ene-4-carboxaldehyde,borneol,α-curcumene,α-bisabolol,cis-caryophyllene,benzyl benzoate,methyl β,β-dimethylbenzenepropanoic acid ester,2,4-decadienal and heneicosane in the essential oil of the five cultivars' Hangjuhua.Among them,juniper camphor is most which were composed of 11.96%,10.51%,10.95%,13.28% and 10.77% of the total essential oil,and methyl β,β-dimethylbenzenepropanoic acid ester is second,which were composed of 1.51%,1.86%,2.52%,4.89% and 2.51% of the total essential oil,respectively.
5种栽培类型杭菊花挥发油中共有成分为1,3,3-三甲基环己-1-烯-4-甲醛、冰片、α-姜黄烯、α-甜没药萜醇、顺式石竹烯、桧脑、安息香酸苄酯、β,β-二甲基苯丙酸甲酯、2,4-癸二烯醛和二十一烷;其中桧脑含量最高,分别占挥发油总量的11.96%,10.51%,10.95%,13.28%和10.77%,为5种栽培类型杭菊花挥发油中最具特征的成分;其次是β,β-二甲基苯丙酸甲酯,分别占挥发油总量的1.51%,1.86%,2.52%,4.89%和2.51%。
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My company can provide pesticide, medicine, veterinary medicine intermediates, have 48 kinds of products (p-Bromo-p-Bromotoluene bromoform 1 - bromo-heptane Triethyl Citrate 1,2,3 - three Bromopropane 3 - Chlorine -4 - fluoro bromobenzene Bromotoluene ethylbenzene 4 - bromo -2 - bromo-ethyl-Chloroaniline 2 - bromo--5 - chloro-toluene 3 - bromo-C methyl 1,6 - dibromo-hexane 1 - bromo --4 - p-methoxy benzaldehyde o-bromo-acetic acid propyl bromide p-fluorotoluene dodecane four bromoethane of iodine bromide toluene tert-butane Tributyl Citrate 2 - bromo-p inter - Hydroxybenzaldehyde bromine butane 2 - bromo-propionic acid bromide veratryl aldehyde inter-bromo-trifluoro-n-hexane of toluene on Bromoxynil Bromotoluene toluene ethylbenzene o-bromophenol bromide Cyclohexane Cyclopentane bran bromate bromide Malay Dibutyl Ethyl Lactate Propylene between bromine bromine bromine between aniline o-anisidine o-fluorophenol difluorobenzonitrile to aminobenzaldehyde Bromotoluene aniline on Bromobenzaldehyde Bromotoluene acid) expressed the hope that customers contact us!
我公司可提供农药,医药,兽药中间体,有四十八种产品(对溴苯酚对溴甲苯溴仿 1-溴庚烷柠檬酸三乙酯 1,2,3-三溴丙烷 3-氯-4-氟溴苯对溴乙苯 4-溴-2-氯苯胺溴乙酸乙酯 2-溴-5-氯甲苯 3-溴丙酸甲酯 1,6-二溴己烷 1-溴-4-硝基苯邻甲氧基苯甲醛溴乙酸丙酯对氟甲苯溴代十二烷对碘甲苯四溴乙烷溴代叔丁烷柠檬酸三丁酯 2-溴氯苯间羟基苯甲醛溴丁烷 2-溴丙酸黎芦醛溴已烷间溴三氟甲苯对溴苯腈对溴乙苯邻溴甲苯溴代环已烷溴代环戊烷糠溴酸马来酸二丁酯溴丙烯乳酸乙酯间溴苯胺间溴苯甲醚邻氟苯酚邻氟苯腈对氨基苯甲醛对溴苯胺对溴苯甲醛对溴苯甲酸)希望广大客户与我司联系!
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The main products are: HH-01 fungicides HH-02 organic dispersant HH-03 cationic starch Wood HH-04 cationic starch Department HH-05 modified starch warp sizing agents also sell German Baker Chemical Co., Ltd. Main Products Defoamer series product: E640, T50 Surface Sizing Agent: A281, A288, K532, pesticides / medicine / veterinary medicine a variety of intermediate products (p-Bromo-p-Bromotoluene bromoform 1 - bromo-heptane triethyl citrate 1,2, 3 - Three Bromopropane 3 - chloro -4 - fluoro bromobenzene Bromotoluene ethylbenzene 4 - bromo -2 - bromo-ethyl-Chloroaniline 2 - bromo--5 - chloro-toluene 3 - bromo-methyl 1,6 C - Dibromo Hexane 1 - bromo -4 - nitrobenzene o-methoxy benzaldehyde acid propyl bromide p-fluorotoluene bromo dodecane toluene four of iodine bromide bromoethane three citric acid tert-butane n-butyl 2 - bromo-p-bromo-butane Hydroxybenzaldehyde between 2 - bromo-propionic acid bromide veratryl aldehyde inter-bromo-trifluoro-n-hexane of toluene on Bromoxynil Bromotoluene toluene ethylbenzene o-bromophenol bromide bromide Cyclohexane Cyclopentane bran acid dibutyl maleate Ethyl Lactate Propylene between bromine bromine bromine between aniline o-anisidine o-fluorophenol difluorobenzonitrile to aminobenzaldehyde Bromotoluene aniline on Bromobenzaldehyde Bromotoluene acid) and other relevant units have been in substantial promotion, and client set up a good relationship of cooperation has been the user's praise.
现主要产品:HH—01杀菌剂 HH—02有机分散剂HH—03阳离子淀粉 HH—04木署阳离子淀粉 HH—05 经纱上浆变性淀粉同时还代理销售德国贝克化学公司系列产品主要产品消泡剂:E640 、T50 表面施胶剂:A281、A288 、K532,农药/医药/兽药中间体多种产品(对溴苯酚对溴甲苯溴仿 1-溴庚烷柠檬酸三乙酯 1,2,3-三溴丙烷 3-氯-4-氟溴苯对溴乙苯 4-溴-2-氯苯胺溴乙酸乙酯 2-溴-5-氯甲苯 3-溴丙酸甲酯 1,6-二溴己烷 1-溴-4-硝基苯邻甲氧基苯甲醛溴乙酸丙酯对氟甲苯溴代十二烷对碘甲苯四溴乙烷溴代叔丁烷柠檬酸三丁酯 2-溴氯苯间羟基苯甲醛溴丁烷 2-溴丙酸黎芦醛溴已烷间溴三氟甲苯对溴苯腈对溴乙苯邻溴甲苯溴代环已烷溴代环戊烷糠溴酸马来酸二丁酯溴丙烯乳酸乙酯间溴苯胺间溴苯甲醚邻氟苯酚邻氟苯腈对氨基苯甲醛对溴苯胺对溴苯甲醛对溴苯甲酸)等在相关单位得到了大量推广,与客户建立了良好的合作关系,得到了用户的赞誉。
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Water,c12-20 acid peg-8 ester,caprylic/capric triglyceride,proplylene glycol,ppg-15 stearyl ether,chondrus crispus,iris germanica(orris extract/cells),centaurea cyanus,macadamia ternifolia,buxus chinensis,triethanolamine,potassium cetyl phosphate,butyrospermum parkii,c12-13 alkyl lactate,carbomer,phenoxyethanol,methylparaben,imidazolidinyl urea,glyceryl hydroxystearin,tocopheryl acetate.retinyl palmitate,sodium hyaluronate,biosaccharide gum-1,propylparaben,disodium edta,ethylparaben,pentadecalactone,hydroxystearic acid,tetradecyloctadecanoic acid,tetradecyleicosanoic acid,hexadecyleicosanoic acid,butylparaben,isobutylparaben,chlorhexidine digluconate,tocopherol,lecithin,ascorbyl palmitate,glyceryl stearate,glyceryl oleate,BHT,citric acid.
水,C12-20 酸 PEG-8酯,辛酸/癸酸三酸甘油酯,丙二醇,PPG-15 硬脂基醚,卡拉胶萃取,德国鸢尾花提取物/细胞,矢车菊提取物,澳洲坚果油,荷荷巴油,三乙醇胺,十六烷基磷酸钾,牛油果,c12-13烷醇乳酸酯,卡波姆,苯氧乙醇,羟苯甲酯,尿素醛,甘油羟基硬脂酸酯,醋酸盐维他命E,维他命A酯,透明质酸钠,多醣物质,羟苯丙酯,乙酸乙二胺二钠,羟苯乙酯,环十五内酯,羟基硬脂酸,十四烷基十八烷酸,十四烷基二十烷酸,十六烷基二十烷酸,羟苯丁酯,对羟基苯甲酸异丁酯,洗必泰葡萄糖酸盐,维生素E,卵磷脂,抗坏血酸棕榈酸酯,甘油硬脂酸,甘油油酸酯,BHT,柠檬酸。水:几乎所有护肤品成分第一位都是水。辛酸/癸酸三酸甘油酯:润滑剂、扩散剂,棕榈油/椰子油衍生物
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Water,decyloleate,propylene glycol,stearic acid,glyceryl stearate,peg-100 stearate,iris germanica(orris extract/cells),chamomilla recutita,arctium majus,prunus dulcis,ceteareth-3, Triethanolamine,phenoxyethanol,methylparaben,imidazolidinyl urea,carbomer,c12-13 alkyl lactate,disodium edta,propylparaben,glyceryl hydroxystearate,cetyl esters,ethylparaben,pentadecalactone,cera microcristallina,trihydroxystearin,butylparaben,hydroxystearic acid,isobutylparaben,chlorhexidine digluconate,tetradecyloctadecanoic acid,tetradecyleicosanoic acid,tocopherol,lecithin,ascorbyl palmitate,glyceryl oleate,citric acid
水,油酸癸酯,丙二醇,硬脂酸,甘油硬脂酸,聚乙二醇硬脂酸酯,鸢尾花提取物/活细胞,洋甘菊萃取,牛蒡提取物,甜杏仁油,鲸蜡硬脂醇醚,三乙醇胺,苯氧乙醇,羟苯甲酯,尿素醛,卡波姆,c12-13烷醇乳酸酯,乙酸乙二胺二钠,羟苯丙酯,甘油羟基硬脂酸酯,十六烷基酯,羟苯乙酯,环十五内酯,微晶蜡,三羟基硬脂精,羟苯丁酯,羟基硬脂酸,对羟基苯甲酸异丁酯,洗必泰葡萄糖酸盐,十四烷基十八烷酸,十四烷基二十烷酸,维生素E ,卵磷脂,抗坏血酸棕榈酸酯,甘油硬脂酸,柠檬酸水:几乎所有护肤品成分第一位都是水。油酸癸酯:滋润、柔肤剂,并常添加于多种化妆品中作为溶剂
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SM6 and SM7 of uncrystal were analyzed through GC-MS, the results showedthat SM6 main contained unsaturated fatty aldehyde with fragrance, i.e.-2,4-decadienal(58%), tetradecanoic acid (55.78%), 2-decenal(50%), Phthalic acid isobutylundecyl ester(47%), 2, 4-Decadienal(41%), 2-Undecenal (31%), 2-Methyl-Z,Z-3, 13-octadecadi-enol(18.84%), and SM7 contained saturation alkanes, i.e. 1, 2-Benzenedicarboxylic acid, butyl cyclohexyl ester(23.90%), Triacontane(22.63%),Nonacosane(21.04%), Heptadecane(18.84%), Octacosane(13.58%). Toxicological experiments were done to insure the pigment safety.
并对紫红丝膜菌色素非晶体部分的黄色油状物SM6和紫色粉末物SM7作了GC-MS分析,结果显示SM6中主要为具有香气成分的不饱和脂肪醛,其中含量较高的依次为:-2,4-癸二烯醛(58%)、十四烷酸(55.78%)、2-癸烯醛(50%)、邻苯二甲酸异丁基十一烷酯(47%)、2,4-癸二烯(41%)、2-十一碳烯醛(31%)、2-甲基-Z,Z-3,13-十八碳二烯酸(18.45%)等;SM7中主要为饱和直链烷烃,其中含量较高的依次为:1,2-苯二羧酸丁基环己酯(23.90%)、三十烷(22.63%)、二十九烷(21.04%)、十七烷(18.84%)、二十八烷(13.58%)。
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Bis-imidazoline was prepared from triethylene tetraamine and N,N-dimethylformamide dimethyl acetal at 85℃ for 2 h with toluene as solvent, with a yield of 90.4%. The reaction of bis-imidazoline with 1,2-dibromoethane and potassium carbonate in acetonitrile provided with a monobromide salt yield of 78.7%. Hydrolysis of monobromide salt under aqueous causic solution formed 1,4,7,10-tetraazzcyclododecane in a 74.2% yield.
用甲苯作溶剂,使三乙烯四胺和N,N-二甲基甲酰胺二甲基缩醛在85℃反应2 h,得到中间体双咪唑啉,产率90.4%,在乙腈溶剂中,碳酸钾存在下,双咪唑啉和1,2-二溴乙烷进行扩环反应,得到环状中间体一溴盐,产率78.7%,一溴盐经碱性水解2 h,得到1,4,7,10-四氮杂十二烷,产率74.2%。
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Thus, in order to attain acetal can be used as precursor of its matrix olefine aldehyde, 2-undecental glycol acetal was synthesized, and the corresponding optimum reaction conditions as: 2-undecental 0.2mol, glycol 0.3mol, cyclohexane as solvent, catalysed by vitamin C, the optium reaction time was 6h, its reaction yield could reach over 77.25%.
为了进一步探求效果更理想的前体化合物,本文继续合成了2-十一烯醛乙二醇缩醛,通过单因素优化实验得到最佳反应条件为:环己烷作溶剂,VC作催化剂,用量0.42%,醛醇物质的量之比0.2:0.3,反应时间6h,此条件下产品收率达77.25%。
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RESULTS: 12 compounds were isolated and identified as aurantiamide acetate (1), aurantiamide benzoate (2), physcion (3), scopoletin (4), vanillin (5), coniferyl aldehyde (6), syringaldehyde (7), syringic acid (8), luteolin (9), apigenin (10), azelaic acid (11), dotriacontanic acid (12), respectively.
结果:从羊耳菊全草的氯仿和乙酸乙酯部分共分离得到12个化合物,分别鉴定为橙黄胡椒酰胺乙酸酯(1),橙黄胡椒酰胺苯甲酸酯(2),大黄素甲醚(3),东莨菪亭(4),香草醛(5),松柏醛(6),丁香醛(7),丁香酸(8),木犀草素(9),芹菜素(10),壬二酸(11),三十二烷酸(12)。
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Also, the type of dispersion of four gasliquid-liquid systems: air-decane-aqueous solution of sodium sulfite and surfactant, airmixture of decane and dodecene-aqueous solution of rhodium complex, ligand, and surfactant, air-mixture of decane, dodecene and tridecyl aldehyde-aqueous solution of rhodium complex, ligand and surfactant, and air-mixture of decane and dodeceneaqueous solution of trisodium salt of tri (m-sulfophenyl) phosphine, and surfactant is determined by electric conductivity.
本文采用电导率测量的方法实验研究了空气—正癸烷—亚硫酸钠和十六烷基三甲基溴化铵水溶液、空气—正癸烷和1-十二碳烯混合物—铑膦络合物催化剂和十六烷基三甲基溴化铵水溶液、空气—正癸烷、1-十二碳烯和十三醛混合物—铑膦络合物催化剂和十六烷基三甲基溴化铵水溶液、空气—正癸烷和1-十二碳烯混合物—三间磺化苯基膦三钠盐和十六烷基三甲基溴化铵水溶液四个三相体系的液液分散特性。当有机相与水相体积比分别为7/3、1/1和3/7时,前三个体系均形成水包油型分散,并有稳定的乳状液生成。
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biguanide; amidinoguanidine:缩二胍;甲脒胍
联甲酰基;甘醛;乙二醛 biformyl; glyoxal | 缩二胍;甲脒胍 biguanide; amidinoguanidine | 联己基;十二烷 bihexyl; dodecane
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dodecanoic acid; lauric acid:十二[烷]酸,月桂酸
十二碳二烯酸 dodecadienoic acid | 十二醛,月桂醛 dodecanal, lauryl aldehyde | 十二[烷]酸,月桂酸 dodecanoic acid, lauric acid
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lauraldehyde:十二醛
launobine 月桂树宾 | lauraldehyde 十二醛 | laurane 月桂烷
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dodecanal; lauraldehyde:十二醛;月桂醛
二环己基胺 dodecahydrodiphenyl-amine; dicyclohexylamine | 十二醛;月桂醛 dodecanal; lauraldehyde | 十二烷 dodecane