- 更多网络例句与二苯甲酰基相关的网络例句 [注:此内容来源于网络,仅供参考]
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A novel monomer the 1-methyl-4,5-bis(4-chlorobenzoy) cyclometer containing cyclohexene were prepared,so a group of novel polys containing the cyclohexene and phthalazinone moieties was prepared by the nucleophilic displacement reaction of 1-methyl-4,5-bis(4-chlorobenzoyl) cyclohexene and 4,4′-dichlorodiphenyl sulfone and 4-(3,5-dimethyl-4-hydroxyphenyl)-2,3-phthalazin-1-one.
用新型聚合单体1-甲基-4,5-二(4-氯代苯甲酰基)环己烯与4-(4-羟基苯基)-2,3-二氮杂萘-1-酮、4,4′-二氯二苯砜单体经亲核共缩聚反应,成功地合成了含环己烯结构的杂环联苯型聚醚系列聚合物。
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Experimental process: jing and 3- methyl -2- methyl ethyl ketonesynthesizes by the benzene zong; Again the glacial acetic acidcatalysis produces 2, 3, 3 - trimethyl - 3H - yinduo; Again has thealkylate response production yinduo iodide after the methyl iodide;The iodide takes off molecular HI under NaOH to become freejier thealkali; Adds 5 - nitryls salicylic aldehydes in the ethyl alcohol forthe solvent under if to respond finally produces 6 '- the nitryl yinduolin spiral benzene and pinan; Through the infrared spectrum andthe ultimate analysis irrevocably proved its structure, and studiedthe annulus with to open the annulus the light to send changes colorthe performance, explained in different solvent medium ultravioletabsorption spectrometry solvent effect, and the comparisondiscoloration the response speed number difference, finally mixed itadds to the methyl methacrylate, the peroxidation benzoin formyl in the plexiglass, tested 6 '- the nitryl yinduolin spiralbenzene and pinan in the glass fatigue resistance, thethermostability.
实验过程:由苯肼和3-甲基-2-丁酮合成腙;再冰醋酸催化生成2 ,3 ,3—三甲基—3H—吲哚;再经过碘甲烷发生烷基化反应生成吲哚碘化物;碘化物在NaOH下脱去一分子HI成为费歇尔碱;在乙醇为溶剂下加5-硝基水杨醛与其反应最后生成6'—硝基吲哚啉螺苯并吡喃;通过红外光谱和元素分析确证其结构,并研究了环体与开环体的光致变色性能,解释了在不同溶剂介质中紫外吸收光谱的溶剂效应,并比较褪色反应速率数的差异,最后将其掺加到甲基丙烯酸甲酯,过氧化二苯甲酰有机玻璃中,测试6'—硝基吲哚啉螺苯并吡喃在玻璃中的抗疲劳性、热稳定性。
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Benzyloxy benzoyldimethylsulfoxide was prepared by the reaction of ethyl 4-benzyloxybenzoate and dimethyl sulfoxide in the presence of sodium hydride, followed by Pummerer reaction with concentrated hydrochloric acid to afford eo-hydroxy-co-thio-methyl-(4/-benzyloxy) acetophenone, which reacted with urea, thiosemicarbazide, semicarbazide hydrochloride and o-phenylenediamine to give imidazolidine-2,4-dione, l,2,4-triazine-3- one and quinoxaline derivatives, respectively.
本文用4-苄氧基苯甲酸乙酯和二甲亚砜为原料,在氢化钠存在下反应,合成了(4′-苄氧基)-苯甲酰基-二甲亚砜。研究了该亚砜在浓盐酸的存在下发生的Pummerer重排反应,用重排产物ω-羟基-ω-甲硫基-(4′-苄氧基)-苯乙酮分别与尿素、氨基脲、氨基硫脲和邻苯二胺反应合成了2,4-咪唑啉-二酮、1,2,4-三嗪-3-酮、喹喔啉等含氮杂环化合物。
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By using the a device being similar to water segregator and by controlling the temperature, cyclization of the intermediate product in chloroform reduced carbonization and gave 2-dodecaneanthraquinane in 68.1% yielding.
以十二烷基苯和苯酐为起始原料,经酰基化、关环和磺化三步反应合成了3-十二烷基蒽醌磺酸;并进一步改进和优化了合成工艺条件:即在催化剂三氯化铝过量50%并有三乙胺存在的条件下,中间体2-(4-十二烷基苯甲酰基)苯甲酸收率为72.45%;关环反应采用氯仿作溶剂,利用类似分水器的装置有效控制反应温度以减少碳化,2-十二烷基蒽醌的收率为68.1%。
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Products: 3 - benzoyl-ethyl acrylate (97% min), acyl phosphorus acid methyl ester (98% min), P acyl three ethyl acetate (98% min), a phosphorus acid acyl The ethyl esters (98% min), 3 - bromine -1,3,4,5 - tetrahydrocannabinol -2 H-1-benzo-Aza Zhuo -2, 1 - naphthalene-tetrahydrocannabinol (98% min), 3,5 - dimethyl benzoyl chloride (99% min), 3,5 - dichloro benzoyl chloride (97% min), the ethyl benzoyl chloride (99% min), a TCA Ester (99.5% min), o-benzoyl methyl benzene (99% min), 4 - phenyl benzophenone (99% min): glacial acetic acid (99% min), methanol (99% min), liquid chlorine (99.5% min), caustic soda (30% min), isopropyl alcohol (99% min), anthranilic acid (99% min), dichloroethane (99% min ), Chunben (99% min), toluene 99% min
3-苯甲酰基丙烯酸乙酯(97%min)、磷酰基乙酸三甲酯(98%min)、磷酰基乙酸三乙酯(98%min)、磷酰基乙酸甲酯二乙酯(98%min)、3-溴-1,3,4,5-四氢-2H-1-苯并氮杂卓-2酮、1-四氢萘酮(98%min)、3,5-二甲基苯甲酰氯(99%min)、3,5-二氯苯甲酰氯(97%min)、对乙基苯甲酰氯(99%min)、氯乙酸甲酯(99.5%min)、邻苯甲酰基苯甲酸甲酯(99%min)、4-苯基二苯甲酮
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Four non-ionic europium complexes,〓-phen(11),〓·bipy(12),〓·dia(13) and 〓(14)(TTA=2-thenoyltrifluoroacetone, DBM=dibenzoylmethane, phen=phenanthroline, bipy=2,2'-bipyridine, dia=4,5- diazafluoren-9-one, dmbp=4,4'-dimethyl-2,2,-bipyridine), were synthesised and the triboluminescent phenomena of 12, 13 and 14 were firstly observed. Structure determinations of 11,12 and 14 were carried out. The triboluminescence maxima of 12 and 13 are similar to those of their photoluminescence. X-Ray structure analyses show that Eu atoms all exhibit eight-coordinate tetragonal antiprismatic geometries and complexes 11, 12 and 14 are all centrosymmetric.
二、合成了四个非离子型的铕的配合物:〓、〓、和〓(14)[HTTA=2-噻吩三氟甲酰丙酮,DBM=二苯甲酰基甲烷,phen=邻菲罗啉, bipy=2,2'-联吡啶,dia=4,5-二氮杂芴-9-酮,dmbp=4,4'-二甲基-2,2'-联吡啶],首次报道了12、13及14的摩擦发光性质,测定了11、12及14的晶体结构,并系统地讨论了晶体结构和摩擦发光活性之间的关系。12及13的摩擦发光光谱的极大值均类似与其相应的光致发光光谱,表明它们有相同的激发态。
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With α-D-glucose as raw material, 3-O-benzoyl-1,2,5,6-O-diisopropylidene-α-D-allofuranose was synthesized by isopropylene protection , oxidation, reduction and benzoylation.
以α-D-葡萄糖为原料,经异丙叉基保护、氧化、还原、苯甲酰化反应合成3-苯甲酰基-1,2,5,6-氧-二异丙叉基-α-D-呋喃阿洛糖。
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Poly with sulfonic acid groups were readily synthesized with biphenol and 1,3-bis(4-fluorobenzoyl)benzene in the presence of excess potassium carbonate followed by sulfonation with chlorosulfonic acid.
以二氯二苯甲烷和2,6-二甲基苯酚为原料合成了含有阻碍基团的双酚单体,用此双酚单体和1,3-二(4-氟苯甲酰基苯)在无水碳酸钾存在的条件下反应制得聚芳醚酮,然后用氯磺酸磺化,控制反应条件,使磺酸基团恰好进入苯环对位,制得新型结构的磺化聚芳醚酮。
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Through condensing o-aminobenzoic acid, ethyl oxalyl chloride and ethylenediamine(or 1,2-propylenediamine), two new ligands N-benzoato-N′-(2- aminoethyl)oxamido(H3oxbe) and N-benzoato-N-(2-amino-2-methylethyl)oxamido(H3oxbt) have been synthesized. Their mononuclear complexes Na·1.5H2O and Na·1.5H2O have also been obtained.
2以邻氨基苯甲酸、草酸乙酯酰氯和乙二胺(或1,2-丙二胺)缩合制得了两种具有不对称草酰胺结构配体N-(2-苯甲酰基)-N&-(2-氨乙基)草酰胺(H3oxbe)和N-(2-苯甲酰基)-N&-(2-氨丙基)草酰胺(H3oxbt),并得到了它们的单核配合物:Na·1.5H2O和Na·1.5H2O。
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In this paper, 4-4-(trifluoromethoxy benzoyl cyclohexyl-3, 5-diaminobenzoate with a large branch chain, pyromellitic dianhydride and 4-(4-aminobenzyl) benzenamine were used to synthesize polyimides. The effect of monomer charge order on pretilt angle was investigated for the first time when PIs were used as LC alignment layer, and the effect of diamine mole ratio on pretilt angle was studied. The thermal stability of the pretilt angle was discussed.
文章用均苯四酸二酐、4,4'-二胺基二苯甲烷和具有较大支链的4-(4-苯甲酰基)环己基-3,5-二胺基苯甲酸酯等单体制备聚酰亚胺,首次研究了单体加料顺序对液晶预倾角的影响,同时也研究了二胺配比对液晶预倾角的影响问题,并探讨了预倾角的热稳定性等问题。
- 更多网络解释与二苯甲酰基相关的网络解释 [注:此内容来源于网络,仅供参考]
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benzyl:苄(基);苯甲酰
benxoyl-苯酰;苯甲酰 | benzyl-苄(基);苯甲酰 | bi-二;双;重
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benzil:苯偶酰
苯偶姻(Benzoin)及其衍生物的结构式如下:苯偶酰(Benzil)又称联苯甲酰、二苯基乙二酮,可光解产生两个苯甲酰自由基,但效率太低,溶解性不好,一般不作光引发剂使用.
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diphenyl diketone; benzil:二苯二甲酮;二苯乙二酮;二苯甲酰
碳酸二苯酯 diphenyl carbonate | 二苯二甲酮;二苯乙二酮;二苯甲酰 diphenyl diketone; benzil | 二苯基二苯氧基硅烷 diphenyl diphenoxysilicane
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diphenylenimide; carbazole; dibenzopyrrole:二亚苯亚胺;咔唑;二苯并吡咯
二伸苯[基]甲醇;9-茀醇 diphenylenecarbinol; 9-flu... | 二亚苯亚胺;咔唑;二苯并吡咯 diphenylenimide; carbazole; dibenzopyrrole | 二苯乙[烷]二酮;二苯草醛;二苯甲酰 diphenylethanedione; diphenylglyoxal; dibe...
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dibenzoyl ketone:二苯甲酰[基]酮;二苯丙三酮
二硫二苯甲酰 dibenzoyl disulfide | 二苯甲酰[基]酮;二苯丙三酮 dibenzoyl ketone | 二苯酰鸟胺酸;鸟尿酸 dibenzoyl ornithine; ornithuric acid
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dibenzoyl disulfide:二硫二苯甲酰
二苯并噻[口+咢][口+井];氧硫蒽 dibenzothioxine; phenoxine | 二硫二苯甲酰 dibenzoyl disulfide | 二苯甲酰[基]酮;二苯丙三酮 dibenzoyl ketone
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formamido:甲酰胺基
亚茀基 fluorenylidene | 甲酰胺基 formamido | 二苯甲[月+潜(之右)]基 formazyl
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formazyl:二苯甲[月+潜(之右)]基
甲酰胺基 formamido | 二苯甲[月+潜(之右)]基 formazyl | 亚胺甲基 formimino
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dibenzoyl ornithine; ornithuric acid:二苯酰鸟胺酸;鸟尿酸
二苯甲酰[基]酮;二苯丙三酮 dibenzoyl ketone | 二苯酰鸟胺酸;鸟尿酸 dibenzoyl ornithine; ornithuric acid | 过氧化二苯甲酰 dibenzoyl peroxide
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tetramethylthiuram disulfide, thiram:二硫化四甲胺硫甲酰基;硫兰
四甲琥珀酸;四甲基丁二酸 tetramethylsuccinic acid | 二硫化四甲胺硫甲酰基;硫兰 tetramethylthiuram disulfide; thiram | 四甲三胺三苯甲烷;胺苯双(二甲胺苯)甲烷 tetramethyltriamino-triphenylmethane