- 更多网络例句与二羧酸相关的网络例句 [注:此内容来源于网络,仅供参考]
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Ethyl 4-[(1-hydroxy-1-methyl)ethyl]-2-propyl-1H-imidazole-5-carboxylate,the key intermediate of Olmesartan ,was synthesized from butanoic acid and o-phenylenediamine via condensation under microwave-irradiation,oxidation,esterification and the Gringard reaction.
用正丁酸与邻苯二胺为原料,在微波照射下缩合成2-丙基苯并咪唑,再氧化开环制得2-丙基咪唑二羧酸,再经酯化、Gringard反应制得抗高血压药物奥美沙坦的关键中间体2-丙基-4-[(1-羟基-1-甲基)乙基]-1H-咪唑-5-羧酸乙酯,总收率32.2%。
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hydantoin was synthesized from diethyl malonate comprising condensation with 1, 2-dichloroethane, ammonolysis to diamide, Hoffmann degradation to give 5-cyclopropanespirohydantoin, and ring-opening with 40% hydrobromic acid.
以丙二酸二乙酯为原料,先与1, 2-二氯乙烷缩合生成1, 1-环丙烷二羧酸二乙酯,再经氨解生成1, 1-环丙烷二甲酰胺,然后在次氯酸钙溶液中进行Hoffmann降解成环生成5-环丙螺海因,最后在40%氢溴酸中开环得到5-溴乙基海因。
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The ammonia was evaporated under decreasing pressure, and the precipitate was filtered off and the liquid was poured into hot saturated picric acid solution to get picrate with a yield of 85.0%. The optimum process starting from imidazole-4,5-dicarboxylic acid was: imidazole-4,5-dicarboxylic acid in acetic anhydride was refluxed to get imidazole-4-carboxylic acid, and the product was esterification in ethanol with a catalyzer of concentrated sulfuric acid to get ethyl imidazole-4-carboxylate, at last the compound above was reduced by LiAlH4 in ether at room temperature to get the target compound, the total yield of this route was 49.6%.
以4,5-二羧酸咪唑为原料的较佳工艺:1 脱羧反应:4,5-二羧酸咪唑40g,醋酐1200ml,回流10h,过滤并将滤液浓缩至干,所得固体加至50%的乙醇溶液回流,过滤并将滤液自然冷却过夜,过滤得固体;2 酯化反应:4(5)-羧酸咪唑50g,乙醇1000ml和浓硫酸60ml,加热回流2h,5%浓度NaOH溶液调节至pH=8,减压浓缩至干,加入少量水回流,自然冷却过夜并过滤得固体;3 还原反应:LiAlH410g,乙醚300ml和4(5)-羧酸咪唑乙酯28g,常温反应1.5h,小心滴加25ml水后过滤,滤渣溶于300ml甲醇中并过滤,收集所得乙醚和甲醇滤液浓缩至干,将所得固体溶于300ml乙醇中加热回流,后将溶液浓缩至约30ml,冷却并过滤得固体,该路线总收率为49.6%。
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We introduce two pyridinedicarboxylate (2,5-H2pdc and 2,6-H2pdc) ligands, under hydrothermal or solvothermal condition, to yield 7 complexes with InCl3. Complex 17 presents a rare example of chiral binodal (4,8)-connected lattice with self-interpenetration.
选择了两种吡啶二羧酸配体: 2,5-吡啶二羧酸(2,5-H2pdc); 2,6-吡啶二羧酸(2,6-H2pdc)和InCl3反应合成了七个配位化合物其中17表现了一例少有的手性的(4,8)连接的双节点自穿插拓扑结构。
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The hNaDCS (human Na+/dicarboxylate cotransporter 3) mediates the transport of Krebs cycle intermediates, such as succinate, citrate and a-ketoglutarate, across the plasma membrane of many epithelial cells.
摘要人钠/二羧酸协同转运蛋白3(human Na~+/dicarboxylate cotransporter3,hNaDC3)基因的编码产物是位于多种上皮细胞膜表面的一类介导琥珀酸、枸橼酸及α-酮戊二酸等三羧酸循环中间产物转运的蛋白。
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Ketoglutaric acid A five-carbon dicarboxylic acid that is an intermediate in the KREBS CYCLE.
酮戊二酸:一种五碳二羧酸,为三羧酸循环的中间产物。
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All the complex series based on 4',4''-dicarboxy-1,6-diphenoxyhex- ane (C6-2COOH) and 4',4''-dicarboxy-1,10-diphenoxydecane (C10-2COOH) possessed higher melting and clearing points, usually showed soft crystal or crystalline smectic phases and crystal polymorphs except C10-2COOH/ p -PhBPy complex displaying also an enantiotropic nematic phase, while the complexes based on 4,4'-dicarboxy-α,ω-diphenoxy tetraethyleneglycol ether (C8O4-2COOH) with a longer flexible spacer exhibited monotropic fluidic smectic SmA and/or nematic phases.
研究表明,分别具有较短的6或10个亚甲基的烷烃间隔基的双苯甲酸衍生物4',4''-二羧酸-1,6-二酚氧基己烷(C6-2COOH)和4',4''-二羧酸-1,10-二酚氧基癸烷(C10-2COOH)的系列复合物具有较高的熔点和清亮点,一般都只出现结晶近晶相和多晶型转变现象。
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SM6 and SM7 of uncrystal were analyzed through GC-MS, the results showedthat SM6 main contained unsaturated fatty aldehyde with fragrance, i.e.-2,4-decadienal(58%), tetradecanoic acid (55.78%), 2-decenal(50%), Phthalic acid isobutylundecyl ester(47%), 2, 4-Decadienal(41%), 2-Undecenal (31%), 2-Methyl-Z,Z-3, 13-octadecadi-enol(18.84%), and SM7 contained saturation alkanes, i.e. 1, 2-Benzenedicarboxylic acid, butyl cyclohexyl ester(23.90%), Triacontane(22.63%),Nonacosane(21.04%), Heptadecane(18.84%), Octacosane(13.58%). Toxicological experiments were done to insure the pigment safety.
并对紫红丝膜菌色素非晶体部分的黄色油状物SM6和紫色粉末物SM7作了GC-MS分析,结果显示SM6中主要为具有香气成分的不饱和脂肪醛,其中含量较高的依次为:-2,4-癸二烯醛(58%)、十四烷酸(55.78%)、2-癸烯醛(50%)、邻苯二甲酸异丁基十一烷酯(47%)、2,4-癸二烯(41%)、2-十一碳烯醛(31%)、2-甲基-Z,Z-3,13-十八碳二烯酸(18.45%)等;SM7中主要为饱和直链烷烃,其中含量较高的依次为:1,2-苯二羧酸丁基环己酯(23.90%)、三十烷(22.63%)、二十九烷(21.04%)、十七烷(18.84%)、二十八烷(13.58%)。
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The amount of Na(superscript +), NH4(superscript +), K(superscript +), Mg(superscript 2+), Ca(superscript 2+), Zn(superscript 2+) in fruits and juice (sports water, green tea , pear juice, carrot juice and carrot and orange juice) were respectively separated and detected by non-suppressed ion chromatography. And pyridine-2, 6-dicarbexylic was used as mobile phase to separated monovalent cations and pyridine-2, 6-dicarbexylic-ethylenedi-amine-oxalic acid was used as mobile phase to separated divalent cations.
采用非抑制型离子色谱法测定了水果以及饮料(运动型饮料、绿茶、水蜜桃汁、胡萝卜汁和胡萝卜橙汁)中Na、NH4、K、Mg(上标 2+)、Ca(上标 2+)、Zn(上标 2+)的含量,其中一价阳离子以吡啶-2,6-二羧酸为淋洗液测定,二价阳离子以吡啶-2,6-二羧酸+乙二胺+草酸为淋洗液测定。
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The amount of Na+, NH4+, K+, Mg2+, Ca2+, Zn2+ in fruits and juice (sports water, green tea , pear juice, carrot juice and carrot and orange juice) were respectively separated and detected by non-suppressed ion chromatography.
采用非抑制型离子色谱法测定了水果以及饮料(运动型饮料、绿茶、水蜜桃汁、胡萝卜汁和胡萝卜橙汁)中Na+、NH4+、K+、Mg2+、Ca2+、Zn2+的含量,其中一价阳离子以吡啶-2,6-二羧酸为淋洗液测定,二价阳离子以吡啶-2,6-二羧酸+乙二胺+草酸为淋洗液测定。
- 更多网络解释与二羧酸相关的网络解释 [注:此内容来源于网络,仅供参考]
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decane dicarboxylic acid:癸烷二羧酸
decalibration 标定降级 | decane dicarboxylic acid 癸烷二羧酸 | decanedioic acid 癸二酸
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tridecane dicarboxylic acid:十三烷二羧酸
tridecandioic acid 十三烷二酸 | tridecane dicarboxylic acid 十三烷二羧酸 | tridecane phosphonic acid 十三烷基膦酸
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azodicarboxylic acid diamide:偶氮二羧酸二酰胺
4-hydroxy-pyrrolidine-2-carboxylic acid4-羟基-2-吡咯烷羧酸 | azodicarboxylic acid diamide偶氮二羧酸二酰胺 | benzenecarboxylic acid苯基羧酸,苯甲酸
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decene dicarboxylic acid:癸烯二羧酸
decelerative force 减速力 | decene dicarboxylic acid 癸烯二羧酸 | decenedioic acid 癸烯二酸
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Biphenyl Dimethyl Dicarboxylate:二羧酸联苯二甲酯
二羥基月桂烯醇 Dihydromyrcenol 85 | 二羧酸聯苯二甲酯 Biphenyl Dimethyl Dicarboxylate | 發光顏料 flush pigment
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dicarboxylic acid:二羧酸
近来提出,瑞氏综合征时血中二羧酸(Dicarboxylic acid)增多是发病的重要原因. 据认为,二羧酸是线粒体功能的抑制物. 瑞氏综合征时,病人血中二羧酸明显增高,且其浓度与血氨增高的水平相关,与病情的严
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dicarboxylic ester:二羧酸酯
dicarboxylic acid 二羧酸 | dicarboxylic ester 二羧酸酯 | dicarfen 地卡芬
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dicarboxylic ester:二元酸酯,二羧酸酯
二元酸,二羧酸 dicarboxylic acid | 二元酸酯,二羧酸酯 dicarboxylic ester | 双核细胞 dicaryon,dikaryon
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heneicosane dicarboxylic acid:二十一烷二羧酸
Henderson process 汉特森法 | heneicosane dicarboxylic acid 二十一烷二羧酸 | heneicosanedioic acid 二十一烷二酸
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pentacosane dicarboxylic acid:二十五烷二羧酸
pentacosandioic acid 二十五烷二酸 | pentacosane dicarboxylic acid 二十五烷二羧酸 | pentacosanoic acid 二十五烷酸