- 更多网络例句与乙酰氨基相关的网络例句 [注:此内容来源于网络,仅供参考]
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In this paper, acetanilide used as start material was chlorosulfonated, then reacted with alkylamines with different length of carbon chain to prepare 4 p-acetylaminophenylsulfonylalkylamine.
本文以乙酰苯胺为起始原料,经氯磺化后分别和不同碳链的正烷基胺反应制得4种不同碳链长度的对乙酰氨基苯磺酰烷基胺,将其水解后制得了对氨基苯磺酰正丁胺、对氨基苯磺酰正辛胺、对氨基苯磺酰正十二胺和对氨基苯磺酰正十八胺。
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We investigated constituent of triterpenoid saponins ofAlbizzia, two new compounds together with two known compounds were isolated from Albizzia julibrissin Durazz. by using column chromatography (macroreticular resin, silica gel, Sephadex gel, reverse phase silica gel),preparative HPLC methods et al.On the basis of spectroscopic analysis, including IR,ESI-MS,~1H-NMR,~(13)C-NMR,HMBC,HMQC,~1H-~1HCOSY and chemical methods, the structure of two new compounds were identified as 3 - O -[β-D-xylopyranosyl(1→2)-β-D-fucopyranosyl (1→6)-β- D -2- deoxy - 2 - acetoamidoglucopyranosyl] -21-O-[(6S)-2- trans- 2,6-dimethyl - 6 - O-β- D - quinovopyranosyl -2,7- octadienoyl] - acacic acid- 28 - O-β-D-glucopyranosyl(1→3)[α-L-arabinofuranosyl(1→4)]-α-L-rhamnopyranosyl(1→2)-β-D-glucopyranoside acacic acid 3- O -β- D- glucopyranosy(1→3)-β- D- fucopyranosl(1→6) [β-D- xylopyranosyl (1→2)]-β-D-glucopyranoside ;two known compounds were acacic acid lactone 3- O -β-D- xylopyranosyl-(1→2)-β-D-fucopyranosl (1→6)- 2-deoxy -2 -acetoamido -β-D- glucopyranoside ; acacic acid lactone 3- O-β-D-xylopyranosyl(1→2)-α-L- arabinopyranosl (1→6)- 2- deoxy - 2- acetoamido -β-D-glucopyranoside . The study lays chemical foundation and chemical reference substance for enhancing quality standard of Albizzia julibrissin Durazz.
本研究论文在综述国内外对合欢属Albizzia三萜皂苷化学成分和药理作用研究进展的基础上,利用传统植化分离手段和现代分离技术,包括大孔树脂、硅胶、葡聚糖凝胶、反相硅胶等柱色谱,制备高效液相色谱法等技术从中药合欢皮中分离得到了4个化合物,其中,2个新化合物和2个己知化合物,并进一步通过现代分析技术IR,ESI-MS,~1H-NMR,~(13C-NMR,HMBC,HMQC,~1H-~1HCOSY等和化学方法鉴定了2个新化合物的结构分别是:3-O-[β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖基]-21-O-[(6S)-2-反式-2,6-二甲基-6-O-β-D-吡喃鸡纳糖基-2,7-辛二烯酸基]-金合欢酸-28-O-α-L-呋喃阿拉伯糖基(1→4)[β-D-吡喃葡萄糖基(1→3)]-α-L-吡喃鼠李糖基(1→2)-β-D-吡喃葡萄糖苷,金合欢酸3-O-β-D-吡喃葡萄糖基(1→3)-β-D-吡喃夫糖基(1→6)[β-D-吡喃木糖基(1→2)]-β-D-吡喃葡萄糖苷;2个已知化合物结构分别是:金和欢酸内酯3-O-β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷,金和欢酸内酯3-O-β-D-吡喃木糖基(1→2)-α-L-吡喃阿拉伯糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷。
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The effects of above-mentionedconditions on alkylene reaction are studied to obtain the optimum reactive conditionsby orthogonal experiments having seven factors and three levels. GCLE is chosen as material to prepare 7-phenyl acetamideyl vinyl cephalkyl acidp-methoxy benyl eatsr in the experiment. The process is as follow: GCLE reacts withiodide in solvent, and produce 3-iodid, then reacts with PPh_3 to produce Witting agent,and reacts with HCHO to produce 7-phenyl acetamideyl vinyl cephalkyl acid p-methoxy benyl eatsr in alkaline conditions.
试验选用GCLE作为原料制备7-苯乙酰氨基-3-乙烯基头孢烷酸对甲氧苄酯,反应过程如下:GCLE与碘化物、PPh3在溶剂中反应生成3位膦盐,在碱性条件下生成Wittig试剂再与HCHO反应生成7-苯乙酰氨基-3-乙烯基头孢烷酸对甲氧苄酯。
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Amino-5-acety laminobenzenesulfonic acid has been synthesized from 2, 5-diaminobenzene sulfonic acid and Acid Red BG (CI Acid Red 37) has been synthesized by coupling the diazonium salt of 2-amino-5-acetylaminobenzenesulfonic acid with racid.
利用2,5-二氨基苯磺酸为原料合成2-氨基-5-乙酰氨基苯磺酸,并进一步经2-氨基-5-乙酰氨基苯磺酸重氮盐与γ酸的偶合反应合成了酸性红BG(CIAcidRed37),并对影响反应的因素进行了讨论
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Methods Starting from 2-chloro-4-nitrophenol and 2- pyridine hydrochlorid, 3-chloro-4-(pyridin-2-ylmethoxy) aniline was obtained via etherization and reduction. The obtained aniline coupled with N-(4-chloro-3-cyano-7-ethoxyquinolin-6-yl) acetamide to give 4-[3-chloro-4-(2-pyridylmethoxy) phenylamino]-3-cyano-7-ethoxy-6-N-acetylaminoquinoline. And then it was deacetylated, followed by reacting with4- but-2-enoyl chloride to yield the target compound neratinib.
以2-氯-4-硝基苯酚和2-氯甲基吡啶为起始原料,经醚化、硝基还原得到3-氯-4-(吡啶-2-甲氧基)苯胺,3-氯-4-(吡啶-2-甲氧基)苯胺与3-氰基-6-乙酰氨基-7-乙氧基-4-氯喹啉反应得到3-氰基-6-乙酰氨基-4-[3-氯-4-(吡啶-2-甲氧基)苯氨基]-7-乙氧基喹啉,3-氰基-6-乙酰氨基-4-[3-氯-4-(吡啶-2-甲氧基)苯氨基]-7-乙氧基喹啉去乙酰保护基后,与-4-二甲氨基-2-丁烯酰氯经酰化反应得到ner-atinib。
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No interference was found with conventional drugs, except vancomycin and methylprednisolone. The average concentrations of phenacetin and paracetarnol were (5.94 ± 4.79) and (8.81 ± 2.91)μg/mL in serum,(3.25 ± 1.10) and (570.45 ± 187.13)μg/mL in urine in the 13 healthy volunteers.
除万古霉素和甲泼尼龙外,其他临床常用药物对测定无干扰。13名健康受试者血清中非那西丁和总对乙酰氨基酚浓度为(5.94±4.79)和(8.81±2.91)μg/mL;尿液中非那西丁和总对乙酰氨基酚浓度为(3.25±1.10)和(570.45±187.13)μg/mL。
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After the diazotization ,2-aminophenol-4-(2-'carboxy)sulfanil phenylamine was coupled with acetoacetanilide,2-naphthol,1-phenyl-3-methyl-5-pyrazolone,1-naphthol-4-sulfonic acid,separately to get the different diazotized compounds,then complexed with potassium chromium sulfate or cobaltous chloride to obtain the yellow,orange,red,purple,blue and other colour dyestuffs.
2-氨基苯酚-4-(2'-羧基)磺酰苯胺重氮化,分别与乙酰乙酰苯胺、2—萘酚、1-苯基-3-甲基-5-吡唑啉酮、尼文酸、1-乙酰氨基-7-萘酚等偶合,得到不同的偶氮化合物,然后分别与硫酸铬或氯化钴进行络合反应,得到黄、橙、红、紫、蓝多种颜色染料,并进行了毛织品的染色实验。
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The invention relates to a synthesis method of N-acetylaminoglucose, which comprises dissolving D-glucosamine hydrochlorate and alcohol at the mass ratio of 2-2.5:100, adjusting the pH value of the solution to 9-10, filtering, taking the filter liquor, mixing and adding acetic anhydride at the 50-60wt% amount of D-glucosamine hydrochlorate, mixing and reacting for 2h, using absolute ethyl alcohol to recrystallizing, filtering and recrystallizing via water, to obtain rod-shape food grade N-acetylaminoglucose.
本发明涉及一种N-乙酰氨基葡萄糖的合成方法。该方法的具体步骤为:将D-葡萄糖胺盐酸盐和乙醇按2~2.5∶100的质量比溶于水中,调节该溶液的pH值为9~10;过滤,取滤液,搅拌下加入乙酸酐,其加入量为原料D-葡萄糖胺盐酸盐量的50~60wt%;搅拌反应2小时后,用无水乙醇进行重结晶;过滤,晶体再用水重结晶,得棒状食品级N-乙酰氨基葡萄糖。
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After basal anesthesia, ilioinguinal/iliohypogastric nerve blockades was administed in nerve block group, paracetamol group received rectal paracetamol, control group had not any medication.
各组患儿行基础麻醉后,神经阻滞组行患侧髂腹股沟/髂腹下神经阻滞;对乙酰氨基酚组经肛门塞人直肠对乙酰氨基酚栓剂;对照组未予任何药物镇痛。
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Results:paracetamol injection solution of 25% was produced through the study on technology.
结果:本实验通过对乙酰氨基酚的工艺研究生产出了25%的对乙酰氨基酚注射剂。
- 更多网络解释与乙酰氨基相关的网络解释 [注:此内容来源于网络,仅供参考]
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acetanilide:乙酰苯胺
乙酰苯胺(acetanilide)是这类药物的母体药物. 1886年Cahn和Hepp两人偶然发现了乙酰苯胺的解热作用.并将其命名为退热冰(antifebrin)作为解热药用. 但发现其毒性过大. 在寻找低毒化合物的过程中,试用了对氨基酚,相信机体能把乙酰苯胺氧化为对氨基酚.
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sodium acetylsalicylate:乙酰水杨酸钠
sodium acetylide 乙炔钠 | sodium acetylsalicylate 乙酰水杨酸钠 | sodium acetylsulfanilate 乙酰氨基苯磺酸钠
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para aminoacet anilide:对氨基乙酰苯胺
para amino salicylic acid 对氨基水杨酸 | para aminoacet anilide 对氨基乙酰苯胺 | para aminoacetophenone 对氨基苯乙酮
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acetamido:乙酰氨基
diethylamino 二乙氨基 -N(C2H5)2 | acetamido 乙酰氨基 -NHCOCH3 | benzyloxycarbonylamino 苄氧羰基氨基 -NHCOOCH2Ar
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acetoamidophenol:[化] 乙酰氨基苯酚
1224acetoacetyl-CoA thiolase[化] 乙酰乙酰辅酶A硫解酶 | 1225acetoamidophenol[化] 乙酰氨基苯酚 | 1226Acetobacter[医] 醋酸杆菌属
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acetylate:乙酰化;乙酰化物
acetyl-glucosamine 乙酰氨基葡萄糖 | acetylate 乙酰化;乙酰化物 | acetylated fat 乙酰(化)脂肪
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acetylizer:乙酰化器
acetylglucosamine 乙酰氨基葡萄糖 | acetylizer 乙酰化器 | acetylmethadol 醋美沙醇
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paracetamol:对乙酰氨基酚
(2) 对乙酰氨基酚(Paracetamol)又称扑热息痛、醋氨酚、必理通等. 其解热作用与阿司匹林相似,但对胃肠道刺激性小. 对阿司匹林过敏及对其副作用不能耐受者可应用本品. 必理通适用于普通感冒引起的头痛、发烧及全身不适.
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PARACETAMOL BP:对乙酰氨基酚
对乙酰氨基酚 Acetaminophen | 对乙酰氨基酚 PARACETAMOL BP98 | 对异丙胺 p-isopopylaniline
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Acetaminophen;Paracetamol:对乙酰氨基酚
对硝苯磷酯 Paraoxone | 对乙酰氨基酚 Acetaminophen;Paracetamol | 对乙氧卡因 Parethoxycaine